Technology Process of 1H-Isoindol-1-one, 2-(4-bromophenyl)-2,3-dihydro-3-hydroxy-3-phenyl-
There total 10 articles about 1H-Isoindol-1-one, 2-(4-bromophenyl)-2,3-dihydro-3-hydroxy-3-phenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(I) oxide; dmap; oxygen;
In
1,2-dichloro-ethane;
at 80 ℃;
for 24h;
under 760.051 Torr;
Sealed tube;
Green chemistry;
DOI:10.1039/d1cc02870g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; water / ethyl acetate / 20 °C
2: 1-fluoro-4-methyl-1,4-diazoniabicyclo<2.2.2>octane ditetrafluoroborate; oxygen; eosin Y / acetonitrile / 6 h / 20 °C / Irradiation
With
eosin Y; water; oxygen; potassium carbonate; 1-fluoro-4-methyl-1,4-diazoniabicyclo<2.2.2>octane ditetrafluoroborate;
In
ethyl acetate; acetonitrile;
DOI:10.1002/chem.201804229
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride / N,N-dimethyl-formamide; dichloromethane / 20 °C / Inert atmosphere
2: potassium carbonate; water / ethyl acetate / 20 °C
3: 1-fluoro-4-methyl-1,4-diazoniabicyclo<2.2.2>octane ditetrafluoroborate; oxygen; eosin Y / acetonitrile / 6 h / 20 °C / Irradiation
With
oxalyl dichloride; eosin Y; water; oxygen; potassium carbonate; 1-fluoro-4-methyl-1,4-diazoniabicyclo<2.2.2>octane ditetrafluoroborate;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201804229