1,2-Dimethylquinolinium methyl sulphate

Base Information

• Chemical Name: 1,2-Dimethylquinolinium methyl sulphate
• CAS No.: 1605-74-9
• Molecular Formula: C12H16NO4S+
• Molecular Weight: 269.321
• Hs Code.: 2933499090
• European Community (EC) Number: 216-518-7
• NSC Number: 97406
• DSSTox Substance ID: DTXSID80166895
• Mol file: 1605-74-9.mol

Synonyms:1,2-Dimethylquinolinium methyl sulphate;1605-74-9;NSC 97406;1-Methylquinaldinium methosulfate;EINECS 216-518-7;1,2-dimethylquinolin-1-ium;methyl sulfate;SCHEMBL382590;C10H9N.C2H6O4S;C11H12N.CH3O4S;1-methylquinaldinium methylsulfate;DTXSID80166895;NSC97406;NSC-97406;AKOS003630971;1,2-Dimethyl quinolinium methylsulphate;C10-H9-N.C2-H6-O4-S;LS-139886

Chemical Property of 1,2-Dimethylquinolinium methyl sulphate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 78.69000
• Density: g/cm³
• LogP: 2.14650
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 269.07217913
• Heavy Atom Count: 18
• Complexity: 246

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=[N+](C2=CC=CC=C2C=C1)C.COS(=O)(=O)[O-]

Technology Process of 1,2-Dimethylquinolinium methyl sulphate

There total 1 articles about 1,2-Dimethylquinolinium methyl sulphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylquinoline (91-63-4) + dimethyl sulfate (77-78-1) → 1,2-dimethyl-quinolinium; methyl sulfate (1605-74-9)

Guidance literature:

With diethyl ether;

DOI:10.1002/hlca.193501801192

Reference yield: 88.0%

2,4,6-triphenylpyrilium perchlorate (1484-88-4,52991-61-4) + 1,2-dimethyl-quinolinium; methyl sulfate (1605-74-9) → 1-methyl-2-(2,4,6-triphenylphenyl)-quinolinium perchlorate

Guidance literature:

With acetic acid; triethylamine; In ethanol; for 2h; Heating;

Reference yield: 87.0%

1,2-dimethyl-quinolinium; methyl sulfate (1605-74-9) + 4-(4-Bromo-phenyl)-2,6-diphenyl-pyranylium; perchlorate → 2-<4-(4-bromophenyl)-2,6-diphenylphenyl>-1-methylquinolinium perchlorate

Guidance literature:

With acetic acid; triethylamine; In ethanol; for 2h; Heating;

upstream raw materials:

2-methylquinoline

dimethyl sulfate

Downstream raw materials:

1-methyl-2-phenylazomethylene-1,2-dihydro-quinoline

1-methyl-2-(3-nitro-trans-styryl)-quinolinium; methyl sulfate

1-methyl-2-(4-nitro-phenylazomethylene)-1,2-dihydro-quinoline

2-(2,4-dinitro-benzylidene)-1-methyl-1,2-dihydro-quinoline