dibenzyl 1-(5-ethoxy-5-oxopentyl)-2-methylhydrazine-1,2-dicarboxylate

Base Information

• Chemical Name: dibenzyl 1-(5-ethoxy-5-oxopentyl)-2-methylhydrazine-1,2-dicarboxylate
• CAS No.: 64377-80-6
• Molecular Formula: C₂₄H₃₀N₂O₆
• Molecular Weight: 442.512

Synonyms:1,2-Hydrazinedicarboxylicacid, 1-(5-ethoxy-5-oxopentyl)-2-methyl-, bis(phenylmethyl) ester (9CI); NSC249988

Chemical Property of dibenzyl 1-(5-ethoxy-5-oxopentyl)-2-methylhydrazine-1,2-dicarboxylate

Chemical Property:

• Vapor Pressure: 1E-11mmHg at 25°C
• Boiling Point: 540°Cat760mmHg
• Flash Point: 280.4°C
• Density: 1.186g/cm³

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of dibenzyl 1-(5-ethoxy-5-oxopentyl)-2-methylhydrazine-1,2-dicarboxylate

There total 1 articles about dibenzyl 1-(5-ethoxy-5-oxopentyl)-2-methylhydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 5-bromovalerate (14660-52-7) + 1-methyl-1,2-dicarbobenzoxy-hydrazine (6002-83-1) → Bis(phenylmethyl)-1-(5-ethoxy-5-oxopentyl)-2-methyl-1,2-hydrazindicarboxylat (64377-80-6)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1002/jps.2600660629

Reference yield:

Bis(phenylmethyl)-1-(5-ethoxy-5-oxopentyl)-2-methyl-1,2-hydrazindicarboxylat (64377-80-6) + isopropylamine (75-31-0) → Bis(phenylmethyl)-1-methyl-2<5-<(1-methylethyl)amino>-5-oxopentyl>-1,2-hydrazindicarboxylat (64377-83-9)

Guidance literature:

Multistep reaction; (i) aq. NaOH, EtOH, (ii) SOCl₂, (iii) /BRN= 605259/, THF;

DOI:10.1002/jps.2600660629

upstream raw materials:

ethyl 5-bromovalerate

1-methyl-1,2-dicarbobenzoxy-hydrazine

Downstream raw materials:

Bis(phenylmethyl)-1-methyl-2<5-<(1-methylethyl)amino>-5-oxopentyl>-1,2-hydrazindicarboxylat

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