5-Methoxychrysene

Base Information

• Chemical Name: 5-Methoxychrysene
• CAS No.: 61413-39-6
• Molecular Formula: C19H14O
• Molecular Weight: 258.33
• Hs Code.: 2909309090
• Mol file: 61413-39-6.mol

Synonyms:5-methoxychryzene;Chrysen-5-yl-methyl-aether;5-Methoxy-chrysen;CHRYSENE,5-METHOXY;chrysen-5-yl-methyl ether;

Chemical Property of 5-Methoxychrysene

Chemical Property:

• Vapor Pressure: 1.57E-08mmHg at 25°C
• Melting Point: 142.5°C
• Refractive Index: 1.4500 (estimate)
• Boiling Point: 469.3°Cat760mmHg
• Flash Point: 193.1°C
• PSA: 9.23000
• Density: 1.197g/cm³
• LogP: 5.15480

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-Methoxychrysene

There total 9 articles about 5-Methoxychrysene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1-methoxy-1-(naphthalen-1-yl)-2-phenylethene (64977-41-9) → 5-methoxychryzene (61413-39-6)

Guidance literature:

With iodine; oxygen; In benzene; Irradiation;

DOI:10.1021/jm00199a007

Reference yield:

(Z)-1-methoxy-1-(naphthalen-1-yl)-2-phenylethene (64977-40-8) → 5-methoxychryzene (61413-39-6)

Guidance literature:

With iodine; oxygen; In benzene; Irradiation;

DOI:10.1021/jm00199a007

Reference yield:

4-methoxyphenanthren (15638-06-9) → 5-methoxychryzene (61413-39-6)

Guidance literature:

Multi-step reaction with 4 steps

1: AlCl₃; nitrobenzene

2: amalgamated zinc; aqueous HCl

3: HF

With hydrogenchloride; aluminium trichloride; amalgamated zinc; hydrogen fluoride; nitrobenzene;

DOI:10.1021/ja01143a006

upstream raw materials:

11-methoxy-3,4-dihydro-2H-chrysen-1-one

chrysen-5-ol

methyl iodide

(E)-1-methoxy-1-(naphthalen-1-yl)-2-phenylethene

Refernces

• 1、 Campbell, J. A.,Grimsrud, E. P.,Hageman, L. R.. "Oxygen Sensitization of Electron Capture Response to Isomers of Polycyclic Aromatic Amines and Hydroxides". . p. 1335 - 1340. Retrieved 2007/10/02.