Benzene, 2,3-bis(dodecyloxy)-1,4-diiodo-

Base Information

Chemical Name:Benzene, 2,3-bis(dodecyloxy)-1,4-diiodo-
CAS No.:378233-26-2
Molecular Formula:C30H52I2O2
Molecular Weight:698.551
Hs Code.:
Mol file:378233-26-2.mol

Synonyms:1,4-diiodo-2,3-di(n-dodecyloxy)benzene;2,3-bis(dodecyloxy)-1,4-diiodobenzene;Benzene,2,3-bis(dodecyloxy)-1,4-diiodo;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 2,3-bis(dodecyloxy)-1,4-diiodo-

Chemical Property:

Melting Point:69-72 °C
Boiling Point:620.0±55.0 °C(Predicted)
PSA：18.46000
Density:1.282±0.06 g/cm3(Predicted)
LogP:11.49520

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, 2,3-bis(dodecyloxy)-1,4-diiodo-

There total 6 articles about Benzene, 2,3-bis(dodecyloxy)-1,4-diiodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 143-15-7
1-dodecylbromide

: 361525-84-0
1,4-diiodo-2,3-dihydroxybenzene

: 378233-26-2
1,4-diiodo-2,3-di(n-dodecyloxy)benzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 5h;
DOI:10.1021/ol0164886

Reference yield: 69.0%

: 112-53-8
1-dodecyl alcohol

: 361525-84-0
1,4-diiodo-2,3-dihydroxybenzene

: 378233-26-2
1,4-diiodo-2,3-di(n-dodecyloxy)benzene

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃; for 1h;
DOI:10.1021/jo061959t

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 378233-26-2
1,4-diiodo-2,3-di(n-dodecyloxy)benzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-BuLi; TMEDA / hexane / 28 h / 20 °C

1.2: 85 percent / hexane / 5 h / -78 - 20 °C

2.1: n-BuLi; TMEDA / hexane / 25 h / 20 °C

2.2: 89 percent / hexane / 5 h / -78 - 20 °C

3.1: 80.9 percent / ICl / CH₂Cl₂ / 0.5 h / 20 °C

4.1: 90 percent / BBr₃ / CH₂Cl₂ / 14 h / 20 °C

5.1: 96 percent / K₂CO₃ / dimethylformamide / 5 h / 120 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; Iodine monochloride; boron tribromide; potassium carbonate; In hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0164886