1-(2-Phenylethyl)-2,3,6-triphenyl-4-piperidinamine

Base Information

• Chemical Name: 1-(2-Phenylethyl)-2,3,6-triphenyl-4-piperidinamine
• CAS No.: 135901-38-1
• Molecular Formula: C31H32N2
• Molecular Weight: 432.5992
• DSSTox Substance ID: DTXSID90929175
• Nikkaji Number: J401.532K
• Mol file: 135901-38-1.mol

Synonyms:BRN 5358687;1-(2-Phenylethyl)-2,3,6-triphenyl-4-piperidinamine;1-(beta-Phenethyl)-2,3,6-triphenyl-4-aminopiperidine;4-Piperidinamine, 1-(2-phenylethyl)-2,3,6-triphenyl-;135901-38-1;4-Piperidinamine, 2,3,6-triphenyl-1-(2-phenylethyl)-;2,3,6-Triphenyl-1-(2-phenylethyl)piperidin-4-amine;DTXSID90929175;LS-113876

Chemical Property of 1-(2-Phenylethyl)-2,3,6-triphenyl-4-piperidinamine

Chemical Property:

• Vapor Pressure: 7.74E-13mmHg at 25°C
• Boiling Point: 566.2°Cat760mmHg
• Flash Point: 279.1°C
• Density: 1.092g/cm³
• XLogP3: 6.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 432.256549029
• Heavy Atom Count: 33
• Complexity: 551

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(C(C(N(C1C2=CC=CC=C2)CCC3=CC=CC=C3)C4=CC=CC=C4)C5=CC=CC=C5)N

Technology Process of 1-(2-Phenylethyl)-2,3,6-triphenyl-4-piperidinamine

There total 1 articles about 1-(2-Phenylethyl)-2,3,6-triphenyl-4-piperidinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

1-(β-phenethyl)-2,3,6-triphenylpiperidin-4-one oxime → 1-(β-phenethyl)-2,3,6-triphenyl-4-aminopiperidine (135901-38-1)

Guidance literature:

With sodium; In ethanol; for 3h; Heating;

DOI:10.1007/BF00772137

Reference yield: 85.0%

benzaldehyde (100-52-7) + 1-(β-phenethyl)-2,3,6-triphenyl-4-aminopiperidine (135901-38-1) → 1-(β-phenethyl)-2,3,6-triphenyl-4-benzylideneaminopiperidine (135901-39-2)

Guidance literature:

With acetic acid; In toluene; for 8h; Heating;

DOI:10.1007/BF00772137

Reference yield:

1-(β-phenethyl)-2,3,6-triphenyl-4-aminopiperidine (135901-38-1) → 1-(β-phenethyl)-2,3,6-triphenyl-4-benzylaminopiperidine (135901-40-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / glacial AcOH / toluene / 8 h / Heating

2: 72 percent / NaBH₄ / ethanol / 3 h

With sodium tetrahydroborate; acetic acid; In ethanol; toluene;

DOI:10.1007/BF00772137

Downstream raw materials:

1-(β-phenethyl)-2,3,6-triphenyl-4-benzylideneaminopiperidine

1-(β-phenethyl)-2,3,6-triphenyl-4-benzylaminopiperidine

1-(β-phenethyl)-2,3,6-triphenyl-4-(N-benzyl-N-propionylamino)piperidine

Refernces