(3,6-Dimethyl-1,2-phenylene)dimethanol

Base Information

Chemical Name:(3,6-Dimethyl-1,2-phenylene)dimethanol
CAS No.:38108-81-5
Molecular Formula:C10H14O2
Molecular Weight:166.22
Hs Code.:
DSSTox Substance ID:DTXSID10529318
Wikidata:Q82399676
Mol file:38108-81-5.mol

Synonyms:38108-81-5;(3,6-Dimethyl-1,2-phenylene)dimethanol;1,2-Bis(hydroxymethyl)-3,6-dimethylbenzene;SCHEMBL3414808;DTXSID10529318;VEUQLUPXQJDUJB-UHFFFAOYSA-N

Suppliers and Price of (3,6-Dimethyl-1,2-phenylene)dimethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of (3,6-Dimethyl-1,2-phenylene)dimethanol

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:166.099379685
Heavy Atom Count:12
Complexity:120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1)C)CO)CO

Technology Process of (3,6-Dimethyl-1,2-phenylene)dimethanol

There total 8 articles about (3,6-Dimethyl-1,2-phenylene)dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 5463-50-3
3,6-dimethyl phthalic anhydride

: 38108-81-5
3,6-dimethyl-1,2-bis(hydroxymethyl)benzene

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 22 - 70 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jacs.9b05570

Reference yield:

: 54598-91-3
4,7-Dimethylphthalide

: 38108-81-5
3,6-dimethyl-1,2-bis(hydroxymethyl)benzene

Guidance literature:: With lithium aluminium tetrahydride; diethyl ether;

Reference yield:

: 625-86-5
2,5-dimethylfuran

: 38108-81-5
3,6-dimethyl-1,2-bis(hydroxymethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 3 h / 20 °C

2: sulfuric acid / 1 h / 0 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 20 h / Reflux

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran; diethyl ether; 1: Diels-Alder reaction;
DOI:10.1246/cl.2010.771