Phosphine oxide, tris(3,5-dimethylphenyl)-

Base Information

Chemical Name:Phosphine oxide, tris(3,5-dimethylphenyl)-
CAS No.:381212-20-0
Molecular Formula:C24H27OP
Molecular Weight:362.44400
Hs Code.:
Mol file:381212-20-0.mol

Synonyms:tris(3,5-dimethylphenyl)phosphine oxide;Phosphine oxide,tris(3,5-dimethylphenyl);(3,5-diMePh)3PO;

Suppliers and Price of Phosphine oxide, tris(3,5-dimethylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Phosphine oxide, tris(3,5-dimethylphenyl)-

Chemical Property:

Boiling Point:559.5±50.0 °C(Predicted)
PSA：26.88000
Density:1.09±0.1 g/cm3(Predicted)
LogP:5.17640

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphine oxide, tris(3,5-dimethylphenyl)-

There total 2 articles about Phosphine oxide, tris(3,5-dimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 69227-47-0
tris(3,5-dimethylphenyl)phosphine

: 381212-20-0
tris(3,5-dimethylphenyl)phosphine oxide

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1002/anie.201809275

Reference yield:

: 556-96-7
5-bromo-1,3-xylene

: 381212-20-0
tris(3,5-dimethylphenyl)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 1 h / Heating

1.2: PCl₃ / diethyl ether / 20 h / 20 °C

2.1: H₂O₂ / CH₂Cl₂

With dihydrogen peroxide; magnesium; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(03)00940-7

Reference yield: 56.0%

: 381212-20-0
tris(3,5-dimethylphenyl)phosphine oxide

: 69227-47-0
tris(3,5-dimethylphenyl)phosphine

Guidance literature:: With 2,6-dimethylpyridine; oxalyl dichloride; hydrogen; tris(2,6-difluorophenyl)borane triethylphosphine oxide; In ⁽²⁾H₈-toluene; at 130 ℃; for 2h; under 3000.3 Torr; Reagent/catalyst;
DOI:10.1002/anie.201809275