(2,3,4,5,6-PENTACHLORO)(2',3',4',5',6'-PENTAFLUORO)BENZIL

Base Information

• Chemical Name: (2,3,4,5,6-PENTACHLORO)(2',3',4',5',6'-PENTAFLUORO)BENZIL
• CAS No.: 38463-15-9
• Molecular Formula: C14Cl5F5O2
• Molecular Weight: 472.40600
• Mol file: 38463-15-9.mol

Synonyms:1.2.3.4.5-Pentafluor-6.7.8.9.10-pentachlorbenzil;2,3,4,5,6-Pentachlorpentafluorbenzil;1-(Perchlorophenyl)-2-(perfluorophenyl)ethane-1,2-dione;1,2,3,4,5-pentafluoro-6,7,8,9,10-pentachlorobenzil;

Chemical Property of (2,3,4,5,6-PENTACHLORO)(2',3',4',5',6'-PENTAFLUORO)BENZIL

Chemical Property:

• PSA: 34.14000
• LogP: 6.71470

Purity/Quality:

99% ^*data from raw suppliers

(2,3,4,5,6-PENTACHLORO)(2',3',4',5',6'-PENTAFLUORO)BENZIL Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,3,4,5,6-PENTACHLORO)(2',3',4',5',6'-PENTAFLUORO)BENZIL

There total 2 articles about (2,3,4,5,6-PENTACHLORO)(2',3',4',5',6'-PENTAFLUORO)BENZIL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

methyl 2-pentachlorophenyl-2-oxo-ethanoate (38449-81-9) + pentafluorophenyl lithium (1076-44-4) → 1-(pentachlorophenyl)-2-(pentafluorophenyl)ethane-1,2-dione (38463-15-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; hexane; reaction at -78°C, 4 hours, hydrolysis with gaseous HCl;;

DOI:10.1039/P19720002464

Reference yield:

→ 1-(pentachlorophenyl)-2-(pentafluorophenyl)ethane-1,2-dione (38463-15-9)

Guidance literature:

Pentachlorbenzylameisensaeuremethylester, Pentafluorphenyl-Li, HCl;

Reference yield: 85.0%

hydrogenchloride (7647-01-0,15364-23-5) + 1-(pentachlorophenyl)-2-(pentafluorophenyl)ethane-1,2-dione (38463-15-9) + pentafluorophenyl lithium (1076-44-4) → di-(pentafluoro phenyl) (perchloro benzoyl) methanol (38449-76-2)

Guidance literature:

In diethyl ether; hexane; reaction at -78°C, 3 hours and hydrolysis with gaseous HCl;;

DOI:10.1039/P19720002469

upstream raw materials:

methyl 2-pentachlorophenyl-2-oxo-ethanoate

pentafluorophenyl lithium

Downstream raw materials:

di-(pentafluoro phenyl) (perchloro benzoyl) methanol

(perchloro benzoic acid) di-(perfluoro phenyl) methyl ester