4-benzoyl-phthalic acid

Base Information

• Chemical Name: 4-benzoyl-phthalic acid
• CAS No.: 3885-88-9
• Molecular Formula: C₁₅H₁₀O₅
• Molecular Weight: 270.241
• Hs Code.: 2918300090
• Mol file: 3885-88-9.mol

Synonyms:4-Benzoyl-phthalsaeure;4-benzoyl-1,2-benzenedicarboxylic acid;1,2-Benzenedicarboxylic acid, 4-benzoyl-;4-Benzoyl-phthalic acid;

Chemical Property of 4-benzoyl-phthalic acid

Chemical Property:

• PSA: 91.67000
• LogP: 2.31400
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Benzoylphthalicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-benzoyl-phthalic acid

There total 18 articles about 4-benzoyl-phthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-xylene (95-47-6) → 4-benzoyl-phthalic acid (3885-88-9)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / nitromethane

2: aq. KMnO₄

With potassium permanganate; aluminium trichloride; In nitromethane;

DOI:10.1139/v78-321

Reference yield:

benzoyl chloride (98-88-4) → 4-benzoyl-phthalic acid (3885-88-9)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / nitromethane

2: aq. KMnO₄

With potassium permanganate; aluminium trichloride; In nitromethane;

DOI:10.1139/v78-321

Reference yield:

benzoyl chloride (98-88-4) → 4-benzoyl-phthalic acid (3885-88-9)

Guidance literature:

Multi-step reaction with 6 steps

1: AlCl₃

2: aqueous HNO₃ / 80 °C

3: sodium sulfide; aqueous ethanol

4: aqueous hydrochloric acid; sodium nitrite / Diazotization_.Erwaermen einer Diazoniumsalz-Loesung mit einer aus Kaliumcyanid, Kupfer(II)-sulfat und Wasser hergestellten Loesung

5: aqueous sulfuric acid

6: aqueous sodium carbonate / anschliessendes Erhitzen mit wss. Kaliumpermanganat-Loesung

With hydrogenchloride; sodium sulfide; aluminium trichloride; ethanol; sulfuric acid; nitric acid; sodium carbonate; sodium nitrite;

upstream raw materials:

5-benzoyl-2-methyl-benzoic acid

4-benzoyl-2-methyl-benzoic acid

(3,4-dimethylphenyl)(phenyl)methanone

4-Methylbenzophenone

Downstream raw materials:

4-benzoyl-phthalic acid-anhydride

Dimethyl-4-benzoylphthalat

2,4-dibenzoyl-benzoic acid

2,5-dibenzoyl-benzoic acid