(2,4-Dichlorophenyl)methyl carbonochloridate

Base Information

Chemical Name:(2,4-Dichlorophenyl)methyl carbonochloridate
CAS No.:39545-38-5
Molecular Formula:C8H5Cl3O2
Molecular Weight:239.485
Hs Code.:
DSSTox Substance ID:DTXSID30535991
Wikidata:Q82410478

Synonyms:(2,4-Dichlorophenyl)methyl carbonochloridate;39545-38-5;SCHEMBL3292219;DTXSID30535991

Suppliers and Price of (2,4-Dichlorophenyl)methyl carbonochloridate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of (2,4-Dichlorophenyl)methyl carbonochloridate

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:237.935512
Heavy Atom Count:13
Complexity:186

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1Cl)Cl)COC(=O)Cl

Technology Process of (2,4-Dichlorophenyl)methyl carbonochloridate

There total 1 articles about (2,4-Dichlorophenyl)methyl carbonochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-44-5
phosgene

: 1777-82-8
(2,4-dichlorophenyl)methanol

: 39545-38-5
C₈H₅Cl₃O₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In diethyl ether;
DOI:10.1016/j.bmcl.2004.08.027

Reference yield: 66.0%

: 6-(tert-butyl)-8-chloro-2,3-dimethylquinolin-4-ol

: 39545-38-5
C₈H₅Cl₃O₂

: 6-(tert-butyl)-8-chloro-2,3-dimethylquinolin-4-yl (2,4-dichlorobenzyl) carbonate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃;
DOI:10.2174/1570180815666180313121735

Reference yield:

: 39545-38-5
C₈H₅Cl₃O₂

: 3-[(S)-2-(2,4-Dichloro-benzyloxycarbonylamino)-3-methyl-butyrylamino]-5-fluoro-4-oxo-pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH

2: EDCI; HOBt; DMAP

3: Dess-Martin periodinane

4: TFA

With dmap; sodium hydroxide; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; 3: Dess-Martin oxidation;
DOI:10.1016/j.bmcl.2004.08.027