2 - Chloro - 6 - hydrazino - 7H - purine

Base Information

• Chemical Name: 2 - Chloro - 6 - hydrazino - 7H - purine
• CAS No.: 5404-88-6
• Molecular Formula: C5H5ClN6
• Molecular Weight: 184.5864
• Hs Code.: 2933990090
• Mol file: 5404-88-6.mol

Synonyms:Purine, 2-chloro-6-hydrazino-;2-chloro-6-hydrazino-9H-purine;2-Chloro-6-hydrazinyl-9H-purine;

Chemical Property of 2 - Chloro - 6 - hydrazino - 7H - purine

Chemical Property:

• Vapor Pressure: 0.000142mmHg at 25°C
• Boiling Point: 332.9°C at 760 mmHg
• Flash Point: 155.1°C
• PSA: 95.74000
• Density: 2.15g/cm³
• LogP: 0.41410
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-6-hydrazino-9H-purine 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2 - Chloro - 6 - hydrazino - 7H - purine

There total 2 articles about 2 - Chloro - 6 - hydrazino - 7H - purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

2,6 dichloropurine (5451-40-1) → 1-(2-chloro-9H-purin-6-yl)hydrazine (5404-88-6)

Guidance literature:

With hydrazine hydrate; In water; for 0.5h; Heating;

DOI:10.1002/chem.200600282

Reference yield:

2,6-dichloro-7H-purine (5451-40-1) → 2-Chloro-6-hydrazino-7H-purine (5404-88-6)

Guidance literature:

With hydrazine;

DOI:10.1021/ja01566a043

Reference yield: 90.0%

4-fluorobenzaldehyde (459-57-4) + 1-(2-chloro-9H-purin-6-yl)hydrazine (5404-88-6) → 2-chloro-6-p-fluorobenzylidenehydrazino-9H-purine (182127-22-6)

Guidance literature:

In 1,4-dioxane;

upstream raw materials:

2,6-dichloro-7H-purine

2,6 dichloropurine

Downstream raw materials:

2-chloro-9H-purine

2-chloro-6-p-chlorobenzylidenehydrazino-9H-purine

2-chloro-6-p-nitrobenzylidenehydrazino-9H-purine

2-chloro-6-p-hydroxybenzylidenehydrazino-9H-purine

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