(2-Benzothiazolylthio)acetic acid ((3-nitrophenyl)methylene)hydrazide

Base Information

Chemical Name:(2-Benzothiazolylthio)acetic acid ((3-nitrophenyl)methylene)hydrazide
CAS No.:94768-91-9
Molecular Formula:C16H12N4O3S2
Molecular Weight:372.4215
Hs Code.:

Synonyms:BRN 5632274;(2-Benzothiazolylthio)acetic acid ((3-nitrophenyl)methylene)hydrazide;ACETIC ACID, (2-BENZOTHIAZOLYLTHIO)-, ((3-NITROPHENYL)METHYLENE)HYDRAZIDE;94768-91-9;C16H12N4O3S2;STK394982;AKOS000606479;C16-H12-N4-O3-S2;2-(1,3-benzothiazol-2-ylsulfanyl)-N'-[(E)-(3-nitrophenyl)methylidene]acetohydrazide;2-(BENZOTHIAZOL-2-YLSULFANYL)-ACETIC ACID (3-NITRO-BENZYLIDENE)-HYDRAZIDE

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-Benzothiazolylthio)acetic acid ((3-nitrophenyl)methylene)hydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.48g/cm³
XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:5
Exact Mass:372.03508260
Heavy Atom Count:25
Complexity:514

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)N=C(S2)SCC(=O)NN=CC3=CC(=CC=C3)[N+](=O)[O-]
Isomeric SMILES:C1=CC=C2C(=C1)N=C(S2)SCC(=O)N/N=C/C3=CC(=CC=C3)[N+](=O)[O-]

Technology Process of (2-Benzothiazolylthio)acetic acid ((3-nitrophenyl)methylene)hydrazide

There total 4 articles about (2-Benzothiazolylthio)acetic acid ((3-nitrophenyl)methylene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 99-61-6
3-nitro-benzaldehyde

: 24044-91-5
[(1,3-benzothiazol-2-ylthio)acetyl]hydrazine

: 94768-91-9
(2-benzothiazolylthio)acetylhydrazone of m-nitrobenzaldehyde

Guidance literature:: In ethanol; for 2h; Heating;
DOI:10.1007/BF00779274

Reference yield:

: 24044-88-0
ethyl 2-(benzo[d]thiazol-2-ylthio)acetate

: 94768-91-9
(2-benzothiazolylthio)acetylhydrazone of m-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / hydrazine hydrate / methanol / 5 h / Heating

2: 79 percent / glacial acetic acid / ethanol / 6 h / Heating

With hydrazine hydrate; acetic acid; In methanol; ethanol;

Reference yield:

: 149-30-4,118090-09-8
2-Mercaptobenzothiazole

: 94768-91-9
(2-benzothiazolylthio)acetylhydrazone of m-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / H₂O; propan-2-ol; dioxane / 1.5 h / 70 °C

2: hydrazine hydrate / H₂O; propan-2-ol; dioxane / 35 °C

3: 58 percent / dioxane / 1.5 h / 50 °C

With potassium hydroxide; hydrazine hydrate; In 1,4-dioxane; water; isopropyl alcohol;
DOI:10.1007/BF01166343