Ribopyranose, 1-deoxy-1-(bis(2-chloroethyl)amino)-, beta-D-

Base Information

• Chemical Name: Ribopyranose, 1-deoxy-1-(bis(2-chloroethyl)amino)-, beta-D-
• CAS No.: 74427-65-9
• Molecular Formula: C9H17 Cl2 N O4
• Molecular Weight: 274.144
• DSSTox Substance ID: DTXSID50225443
• Wikidata: Q76155610
• Mol file: 74427-65-9.mol

Synonyms:ICIG 1490;Ribopyranose, 1-deoxy-1-(bis(2-chloroethyl)amino)-, beta-D-;BRN 5510748;74427-65-9;1-Deoxy-1-(bis(2-chloroethyl)amino)-beta-D-ribopyranose;(Bis(chloro-2 ethyl)amino)-1-desoxy-1 beta-D-ribopyrannose [French];(Bis(chloro-2 ethyl)amino)-1-desoxy-1 beta-D-ribopyrannose;C9H17Cl2NO4;C9-H17-Cl2-N-O4;DTXSID50225443;LS-143796

Chemical Property of Ribopyranose, 1-deoxy-1-(bis(2-chloroethyl)amino)-, beta-D-

Chemical Property:

• Vapor Pressure: 5.72E-07mmHg at 25°C
• Boiling Point: 369.6°C at 760 mmHg
• Flash Point: 177.4°C
• PSA: 73.16000
• Density: 1.44g/cm³
• LogP: -0.79500
• XLogP3: -0.6
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 273.0534634
• Heavy Atom Count: 16
• Complexity: 204

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(C(C(C(O1)N(CCCl)CCCl)O)O)O
• Isomeric SMILES: C1[C@H]([C@H]([C@H]([C@@H](O1)N(CCCl)CCCl)O)O)O

Technology Process of Ribopyranose, 1-deoxy-1-(bis(2-chloroethyl)amino)-, beta-D-

There total 1 articles about Ribopyranose, 1-deoxy-1-(bis(2-chloroethyl)amino)-, beta-D- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.5%

D-ribose (10257-32-6) + N,N-bis(chloro-2-ethyl)amine (334-22-5) → -1-desoxy-1-β-D-ribopyrannose (74427-65-9)

Guidance literature:

In acetone; for 0.25h; Heating;

Reference yield: 68.0%

acetic anhydride (108-24-7) + -1-desoxy-1-β-D-ribopyrannose (74427-65-9) → tri-O-acetyl-2,3,4 -1-desoxy-1 β-D-rybopyrannose (74427-66-0)

Guidance literature:

With pyridine; 1.) 0 deg C, 12 h; 2.) water, rt, 1h;

upstream raw materials:

D-ribose

N,N-bis(chloro-2-ethyl)amine

Downstream raw materials:

tri-O-acetyl-2,3,4 -1-desoxy-1 β-D-rybopyrannose

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