10-Oxa-2,6,8-triazadodec-7-enoic acid, 7-[[(1,1-dimethylethoxy)carbonyl]amino]-6,11,11-trimethyl-9-oxo-3-[2-ox o-2-[(phenylmethyl)amino]ethyl]-, phenylmethyl ester, (3S)-

Base Information

Chemical Name:10-Oxa-2,6,8-triazadodec-7-enoic acid, 7-[[(1,1-dimethylethoxy)carbonyl]amino]-6,11,11-trimethyl-9-oxo-3-[2-ox o-2-[(phenylmethyl)amino]ethyl]-, phenylmethyl ester, (3S)-
CAS No.:400053-91-0
Molecular Formula:C32H45N5O7
Molecular Weight:611.739
Hs Code.:

10-Oxa-2,6,8-triazadodec-7-enoic acid,
7-[[(1,1-dimethylethoxy)carbonyl]amino]-6,11,11-trimethyl-9-oxo-3-[2-ox
o-2-[(phenylmethyl)amino]ethyl]-, phenylmethyl ester, (3S)-

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Chemical Property of 10-Oxa-2,6,8-triazadodec-7-enoic acid, 7-[[(1,1-dimethylethoxy)carbonyl]amino]-6,11,11-trimethyl-9-oxo-3-[2-ox o-2-[(phenylmethyl)amino]ethyl]-, phenylmethyl ester, (3S)-

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Technology Process of 10-Oxa-2,6,8-triazadodec-7-enoic acid, 7-[[(1,1-dimethylethoxy)carbonyl]amino]-6,11,11-trimethyl-9-oxo-3-[2-ox o-2-[(phenylmethyl)amino]ethyl]-, phenylmethyl ester, (3S)-

There total 11 articles about 10-Oxa-2,6,8-triazadodec-7-enoic acid, 7-[[(1,1-dimethylethoxy)carbonyl]amino]-6,11,11-trimethyl-9-oxo-3-[2-ox o-2-[(phenylmethyl)amino]ethyl]-, phenylmethyl ester, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 145013-05-4
tert-butyl N-({[(tert-butoxy)carbonyl]amino}methanethioyl)carbamate

: [(S)-1-(Benzylcarbamoyl-methyl)-3-methylamino-propyl]-carbamic acid benzyl ester

: 400053-91-0
C₃₂H₄₅N₅O₇

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide;
DOI:10.1055/s-2001-18108

Reference yield:

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: [(S)-1-(Benzylcarbamoyl-methyl)-3-methylamino-propyl]-carbamic acid benzyl ester

: 400053-91-0
benzyl-(3S)-3-benzyloxycarbonylamino-5-(N-methyl-bis-tert-butoxycarbonylguanidyl)pentanamide

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;
DOI:10.1002/chem.200305358

Reference yield:

: 77856-52-1
(S)-3-<(benzyloxycarbonyl)amino>-4-(methoxycarbonyl)butyric acid

: 400053-91-0
benzyl-(3S)-3-benzyloxycarbonylamino-5-(N-methyl-bis-tert-butoxycarbonylguanidyl)pentanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: BH₃ / tetrahydrofuran / 4 h / -10 - 20 °C

2.1: Me₃Al / hexane; benzene / 1.08 h / -10 - 20 °C

2.2: 1.10 g / hexane; benzene / 2.33 h / 0 - 20 °C

3.1: 83 percent / diethyl azodicarboxylate; Bu₃P / tetrahydrofuran / 2.33 h / 20 °C

4.1: PhSH; Cs₂CO₃ / acetonitrile / 20 °C

5.1: 412 mg / Et₃N; HgCl₂ / dimethylformamide / 2 h / 0 °C

With tributylphosphine; borane; trimethylaluminum; caesium carbonate; thiophenol; triethylamine; mercury dichloride; diethylazodicarboxylate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1002/chem.200305358