1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID

Base Information

Chemical Name:1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID
CAS No.:400653-36-3
Molecular Formula:C13H14N2O4
Molecular Weight:262.26100
Hs Code.:
Mol file:400653-36-3.mol

Synonyms:1-t-Butyloxycarbonylbenzimidazole-5-carboxylic Acid;benzimidazol-1,5-dicarboxylic acid 1-tert-butyl ester;1-BOC-benzimidazole-5-carboxilic acid;

Suppliers and Price of 1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID 95.00%
5MG
$ 503.88

Total 5 raw suppliers

Chemical Property of 1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID

Chemical Property:

PSA：81.42000
LogP:2.51770

Purity/Quality:

98% ^*data from raw suppliers

1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID

There total 2 articles about 1-BOC-BENZIMIDAZOLE-5-CARBOXILIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 15788-16-6
5-benzimidazolecarboxylic acid

: 400653-36-3
1-{[(1,1-dimethylethyl)oxy]carbonyl}-1H-benzimidazole-5-carboxylic acid

Guidance literature:: With sodium carbonate; In 1,4-dioxane; water; at 0 - 20 ℃;
DOI:10.1016/S0968-0896(02)00268-7

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 15788-16-6
5-benzimidazolecarboxylic acid

: C₁₃H₁₄N₂O₄

: 400653-36-3
1-{[(1,1-dimethylethyl)oxy]carbonyl}-1H-benzimidazole-5-carboxylic acid

Guidance literature:: In N,N-dimethyl-formamide; for 24h;

Reference yield:

: 1159822-27-1
1-Cbz-3-aminopyrrolidine hydrochloride

: 400653-36-3
1-{[(1,1-dimethylethyl)oxy]carbonyl}-1H-benzimidazole-5-carboxylic acid

: 400653-37-4
1-Cbz-3-[[1-(t-butyloxycarbonyl)benzimidazol-5-yl]-carbonyl]aminopyrrolidine

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 24h;