4-TERT-BUTYL-2,6-DIMETHYLPHENYLMAGNESIUM BROMIDE

Base Information

• Chemical Name: 4-TERT-BUTYL-2,6-DIMETHYLPHENYLMAGNESIUM BROMIDE
• CAS No.: 400656-18-0
• Molecular Formula: C12H17BrMg
• Molecular Weight: 265.47200
• Mol file: 400656-18-0.mol

Synonyms:4-tert-Butyl-2,6-dimethylphenylmagnesium bromide 0.5 M in Tetrahydrofuran;Magnesium,bromo[4-(1,1-dimethylethyl)-2,6-dimethylphenyl];(4-(tert-butyl)-2,6-dimethylphenyl)magnesium bromide;4-t-butyl-2,6-dimethylphenylmagnesium bromide;

Chemical Property of 4-TERT-BUTYL-2,6-DIMETHYLPHENYLMAGNESIUM BROMIDE

Chemical Property:

• PSA: 0.00000
• LogP: 4.24670

Purity/Quality:

97% ^*data from raw suppliers

4-tert-Butyl-2,6-dimethylphenylmagnesiumbromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-TERT-BUTYL-2,6-DIMETHYLPHENYLMAGNESIUM BROMIDE

There total 2 articles about 4-TERT-BUTYL-2,6-DIMETHYLPHENYLMAGNESIUM BROMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-t-butyl-2,6-dimethylbromobenzene (5345-05-1) → (4-(tert-butyl)-2,6-dimethylphenyl)magnesium bromide (400656-18-0)

Guidance literature:

With magnesium; In tetrahydrofuran; for 2h; Heating;

DOI:10.1016/S0040-4020(01)85691-X

Reference yield:

5-tert-Butyl-m-xylene (98-19-1) → (4-(tert-butyl)-2,6-dimethylphenyl)magnesium bromide (400656-18-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / bromine, iron filings / CCl₄

2: 95 percent / Mg / tetrahydrofuran / 2 h / Heating

With bromine; iron; magnesium; In tetrahydrofuran; tetrachloromethane;

DOI:10.1016/S0040-4020(01)85691-X

Reference yield: 75.0%

(4-(tert-butyl)-2,6-dimethylphenyl)magnesium bromide (400656-18-0) → C24H34Se

Guidance literature:

With selenium(II) chloride; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1016/j.tetlet.2004.11.125

upstream raw materials:

4-t-butyl-2,6-dimethylbromobenzene

5-tert-Butyl-m-xylene

Downstream raw materials:

bis(4-tert-butyl-2,6-dimethylphenyl) disulfide

C₂₆H₃₂N₂O₄S₃

3,3''-((1E,1'E)-(1,2-phenylenebis(azanylylidene))bis(methanylylidene))bis(4'-(tertbutyl)-2',5,6'-trimethyl-[1,1'-biphenyl]-2-ol)

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