Benzenemethanol, 2,6-dibromo-4-(1,1-dimethylethyl)-a-[4-(1,1-dimethylethyl)-2,6-dimethyl phenyl]-

Base Information

Chemical Name:Benzenemethanol, 2,6-dibromo-4-(1,1-dimethylethyl)-a-[4-(1,1-dimethylethyl)-2,6-dimethyl phenyl]-
CAS No.:400656-19-1
Molecular Formula:C23H30Br2O
Molecular Weight:482.299
Hs Code.:

Synonyms:

Suppliers and Price of Benzenemethanol, 2,6-dibromo-4-(1,1-dimethylethyl)-a-[4-(1,1-dimethylethyl)-2,6-dimethyl phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzenemethanol, 2,6-dibromo-4-(1,1-dimethylethyl)-a-[4-(1,1-dimethylethyl)-2,6-dimethyl phenyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzenemethanol, 2,6-dibromo-4-(1,1-dimethylethyl)-a-[4-(1,1-dimethylethyl)-2,6-dimethyl phenyl]-

There total 1 articles about Benzenemethanol, 2,6-dibromo-4-(1,1-dimethylethyl)-a-[4-(1,1-dimethylethyl)-2,6-dimethyl phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 5345-05-1
4-t-butyl-2,6-dimethylbromobenzene

: 350577-89-8
4-tert-butyl-2,6-dibromobenzaldehyde

: 400656-19-1
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methanol

Guidance literature:: 4-t-butyl-2,6-dimethylbromobenzene; With iodine; magnesium; In diethyl ether; for 3h; Heating;

4-tert-butyl-2,6-dibromobenzaldehyde; In diethyl ether; for 3h; Further stages.; Heating;
DOI:10.1021/ja010658s

Reference yield: 90.0%

: 400656-19-1
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methanol

: 400656-20-4
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)chloromethane

Guidance literature:: With thionyl chloride; at 20 ℃;
DOI:10.1021/ja010658s

Reference yield:

: 400656-19-1
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methanol

: 400655-84-7
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)diazomethane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / SOCl₂ / 20 °C

2: 93 percent / AgBF₄ / dioxane / 100 °C

3: 91 percent / NaNO₂ / acetic acid; acetic anhydride / 20 °C

4: 17.7 percent / t-BuOK / 2-methyl-propan-2-ol / 20 °C

With silver tetrafluoroborate; thionyl chloride; potassium tert-butylate; sodium nitrite; In 1,4-dioxane; acetic anhydride; acetic acid; tert-butyl alcohol;
DOI:10.1021/ja010658s