ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Base Information

Chemical Name:ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate
CAS No.:400656-22-6
Molecular Formula:C₂₆H₃₄Br₂N₂O₃
Molecular Weight:582.376
Hs Code.:

Synonyms:ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Suppliers and Price of ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

There total 5 articles about ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 400656-21-5
ethyl N-[2,6-dibromo-4-tert-butylphenyl][2,6-dimethyl-4-tert-butylphenyl]-methylcarbamate

: 400656-22-6
ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Guidance literature:: With sodium nitrite; In acetic anhydride; acetic acid; at 20 ℃;
DOI:10.1021/ja010658s

Reference yield:

: 400656-20-4
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)chloromethane

: 400656-22-6
ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / AgBF₄ / dioxane / 100 °C

2: 91 percent / NaNO₂ / acetic acid; acetic anhydride / 20 °C

With silver tetrafluoroborate; sodium nitrite; In 1,4-dioxane; acetic anhydride; acetic acid;
DOI:10.1021/ja010658s

Reference yield:

: 400656-19-1
(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methanol

: 400656-22-6
ethyl N-nitroso-N-(2,6-dibromo-4-tert-butylphenyl)(2,6-dimethyl-4-tert-butylphenyl)methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / SOCl₂ / 20 °C

2: 93 percent / AgBF₄ / dioxane / 100 °C

3: 91 percent / NaNO₂ / acetic acid; acetic anhydride / 20 °C

With silver tetrafluoroborate; thionyl chloride; sodium nitrite; In 1,4-dioxane; acetic anhydride; acetic acid;
DOI:10.1021/ja010658s