4H-1,3,2-Benzodioxaphosphorin, 4,4-bis(trifluoromethyl)-2-[2,2,2-trifluoro-1-[2-(phenylmethoxy)phenyl]-1-( trifluoromethyl)ethoxy]-, 2-oxide

Base Information

Chemical Name:4H-1,3,2-Benzodioxaphosphorin, 4,4-bis(trifluoromethyl)-2-[2,2,2-trifluoro-1-[2-(phenylmethoxy)phenyl]-1-( trifluoromethyl)ethoxy]-, 2-oxide
CAS No.:400713-17-9
Molecular Formula:C25H15F12O5P
Molecular Weight:654.346
Hs Code.:

4H-1,3,2-Benzodioxaphosphorin,
4,4-bis(trifluoromethyl)-2-[2,2,2-trifluoro-1-[2-(phenylmethoxy)phenyl]-1-(
trifluoromethyl)ethoxy]-, 2-oxide

Synonyms:

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Chemical Property of 4H-1,3,2-Benzodioxaphosphorin, 4,4-bis(trifluoromethyl)-2-[2,2,2-trifluoro-1-[2-(phenylmethoxy)phenyl]-1-( trifluoromethyl)ethoxy]-, 2-oxide

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Technology Process of 4H-1,3,2-Benzodioxaphosphorin, 4,4-bis(trifluoromethyl)-2-[2,2,2-trifluoro-1-[2-(phenylmethoxy)phenyl]-1-( trifluoromethyl)ethoxy]-, 2-oxide

There total 1 articles about 4H-1,3,2-Benzodioxaphosphorin, 4,4-bis(trifluoromethyl)-2-[2,2,2-trifluoro-1-[2-(phenylmethoxy)phenyl]-1-( trifluoromethyl)ethoxy]-, 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 836-78-2
2-[2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl]phenol

: 151039-03-1
2-(2-benzyloxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol

: 400713-17-9
2-[1-(2-benzyloxy-phenyl)-2,2,2-trifluoro-1-trifluoromethyl-ethoxy]-4,4-bis-trifluoromethyl-4H-benzo[1,3,2]dioxaphosphinine 2-oxide

Guidance literature:: 2-(2-benzyloxyphenyl)-1,1,1,3,3,3-hexafluoropropan-2-ol; With phosphorus trichloride;

2-[2,2,2-trifluoro-1-hydroxy-1-(trifluoromethyl)ethyl]phenol;

With 3,3-dimethyldioxirane; Further stages.;
DOI:10.1021/ol016941d

Reference yield:

: 400713-17-9
2-[1-(2-benzyloxy-phenyl)-2,2,2-trifluoro-1-trifluoromethyl-ethoxy]-4,4-bis-trifluoromethyl-4H-benzo[1,3,2]dioxaphosphinine 2-oxide

: 400713-14-6
1,1,1,3,3,3-hexafluoro-2-[2-(2-oxo-4,4-bis-trifluoromethyl-4H-2λ⁵-benzo[1,3,2]dioxaphosphinin-2-yloxy)-phenyl]-propan-2-ol

: 2-[2,2,2-trifluoro-1-(2-oxo-4,4-bis-trifluoromethyl-4H-2λ⁵-benzo[1,3,2]dioxaphosphinin-2-yloxy)-1-trifluoromethyl-ethyl]-phenol

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; for 0.166667h; under 760.051 Torr;
DOI:10.1021/ol016941d

Reference yield:

: 400713-17-9
2-[1-(2-benzyloxy-phenyl)-2,2,2-trifluoro-1-trifluoromethyl-ethoxy]-4,4-bis-trifluoromethyl-4H-benzo[1,3,2]dioxaphosphinine 2-oxide

: 400713-14-6
1,1,1,3,3,3-hexafluoro-2-[2-(2-oxo-4,4-bis-trifluoromethyl-4H-2λ⁵-benzo[1,3,2]dioxaphosphinin-2-yloxy)-phenyl]-propan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / tetrahydrofuran / 0.17 h / 20 °C / 760.05 Torr

With hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/ol016941d