tert-butyl 4-acetaMidobenzylcarbaMate

Base Information

• Chemical Name: tert-butyl 4-acetaMidobenzylcarbaMate
• CAS No.: 401573-23-7
• Molecular Formula: C14H20N2O3
• Molecular Weight: 264.324
• Mol file: 401573-23-7.mol

Synonyms:tert-butyl 4-acetaMidobenzylcarbaMate;

Chemical Property of tert-butyl 4-acetaMidobenzylcarbaMate

Chemical Property:

• PSA: 67.43000
• LogP: 3.13360
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl4-acetamidobenzylcarbamate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl 4-acetaMidobenzylcarbaMate

There total 4 articles about tert-butyl 4-acetaMidobenzylcarbaMate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

acetyl chloride (75-36-5) + tert-butyl (4-aminobenzyl)carbamate (94838-55-8) → tert-butyl N-[(4-acetylamino)benzyl]carbamate (401573-23-7)

Guidance literature:

With pyridine; at 20 ℃; for 16h;

DOI:10.1021/jm030089u

Reference yield:

(4-aminomethyl)aniline (4403-71-8) → tert-butyl N-[(4-acetylamino)benzyl]carbamate (401573-23-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / tetrahydrofuran / 2 h / 20 °C

2: 96 percent / pyridine / 16 h / 20 °C

With pyridine; In tetrahydrofuran;

DOI:10.1021/jm030089u

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → tert-butyl N-[(4-acetylamino)benzyl]carbamate (401573-23-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / tetrahydrofuran / 2 h / 20 °C

2: 96 percent / pyridine / 16 h / 20 °C

With pyridine; In tetrahydrofuran;

DOI:10.1021/jm030089u

upstream raw materials:

acetyl chloride

tert-butyl (4-aminobenzyl)carbamate

di-tert-butyl dicarbonate

(4-aminomethyl)aniline

Downstream raw materials:

(4-acetamidophenyl)methanammonium chloride

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