Silane, (1,1-dimethylethyl)[[6-[(1R,2E,3R)-2-[2-[[(1,1-dimethylethyl)dimethylsilyl] oxy]ethylidene]-3-[1-(methoxymethoxy)-1-methylethyl]-1-methylcyclopent yl]-4-methylene-6-(phenylsulfonyl)hexyl]oxy]diphenyl-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)[[6-[(1R,2E,3R)-2-[2-[[(1,1-dimethylethyl)dimethylsilyl] oxy]ethylidene]-3-[1-(methoxymethoxy)-1-methylethyl]-1-methylcyclopent yl]-4-methylene-6-(phenylsulfonyl)hexyl]oxy]diphenyl-
CAS No.:401593-47-3
Molecular Formula:C48H72O6SSi2
Molecular Weight:833.333
Hs Code.:

Silane,
(1,1-dimethylethyl)[[6-[(1R,2E,3R)-2-[2-[[(1,1-dimethylethyl)dimethylsilyl]
oxy]ethylidene]-3-[1-(methoxymethoxy)-1-methylethyl]-1-methylcyclopent
yl]-4-methylene-6-(phenylsulfonyl)hexyl]oxy]diphenyl-

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Chemical Property of Silane, (1,1-dimethylethyl)[[6-[(1R,2E,3R)-2-[2-[[(1,1-dimethylethyl)dimethylsilyl] oxy]ethylidene]-3-[1-(methoxymethoxy)-1-methylethyl]-1-methylcyclopent yl]-4-methylene-6-(phenylsulfonyl)hexyl]oxy]diphenyl-

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Technology Process of Silane, (1,1-dimethylethyl)[[6-[(1R,2E,3R)-2-[2-[[(1,1-dimethylethyl)dimethylsilyl] oxy]ethylidene]-3-[1-(methoxymethoxy)-1-methylethyl]-1-methylcyclopent yl]-4-methylene-6-(phenylsulfonyl)hexyl]oxy]diphenyl-

There total 9 articles about Silane, (1,1-dimethylethyl)[[6-[(1R,2E,3R)-2-[2-[[(1,1-dimethylethyl)dimethylsilyl] oxy]ethylidene]-3-[1-(methoxymethoxy)-1-methylethyl]-1-methylcyclopent yl]-4-methylene-6-(phenylsulfonyl)hexyl]oxy]diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 401593-29-1
tert-butyl-(4-iodomethyl-pent-4-enyloxy)-diphenyl-silane

: 401593-28-0
{2-[(2R,5R)-2-Benzenesulfonylmethyl-5-(1-methoxymethoxy-1-methyl-ethyl)-2-methyl-cyclopent-(E)-ylidene]-ethoxy}-tert-butyl-dimethyl-silane

: 401593-47-3
C₄₈H₇₂O₆SSi₂

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/S0040-4039(01)02032-9

Reference yield:

: 1071-73-4
5-Hydroxy-2-pentanone

: 401593-47-3
C₄₈H₇₂O₆SSi₂

Guidance literature:: Multi-step reaction with 5 steps

1: Ca(COCl)2; CO₂

2: NaI

3: 82 percent / KHMDS / tetrahydrofuran / 0 °C

With carbon dioxide; Ca(COCl)2; potassium hexamethylsilazane; sodium iodide; In tetrahydrofuran; 2: Wittig reaction;
DOI:10.1016/S0040-4039(01)02032-9

Reference yield:

: 131085-31-9
5-((tert-butyldiphenylsilyl)oxy)pentan-2-one

: 401593-47-3
C₄₈H₇₂O₆SSi₂

Guidance literature:: Multi-step reaction with 4 steps

1: Ca(COCl)2; CO₂

2: NaI

3: 82 percent / KHMDS / tetrahydrofuran / 0 °C

With carbon dioxide; Ca(COCl)2; potassium hexamethylsilazane; sodium iodide; In tetrahydrofuran; 1: Wittig reaction;
DOI:10.1016/S0040-4039(01)02032-9