N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide

Base Information

• Chemical Name: N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide
• CAS No.: 115062-74-3
• Molecular Formula: C₁₅H₁₂N₂O₂
• Molecular Weight: 252.272
• Mol file: 115062-74-3.mol

Synonyms:N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide

Chemical Property of N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide

Chemical Property:

• Vapor Pressure: 1.27E-07mmHg at 25°C
• Boiling Point: 430.7°Cat760mmHg
• PKA: 0.47±0.20(Predicted)
• Flash Point: 214.3°C
• PSA: 50.27000
• Density: 1.31g/cm³
• LogP: 2.56400

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide

There total 2 articles about N-(2,6-dimethylphenyl)-2,3-pyridinedicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2,3-pyridinedicarboximide (4664-00-0,303983-78-0) + 2,6-dimethylaniline (87-62-7) → 6-(2,6-Dimethyl-phenyl)-pyrrolo[3,4-b]pyridine-5,7-dione (115062-74-3)

Guidance literature:

With triethylamine; 3-diphenyloxyphosphinyl-2-oxazolidinone; In acetonitrile; at 40 ℃; for 0.75h;

DOI:10.1016/j.ejmech.2006.12.003

Reference yield: 70.0%

Pyridine-2,3-dicarboxylic anhydride (699-98-9) + 2,6-dimethylaniline (87-62-7) → 6-(2,6-Dimethyl-phenyl)-pyrrolo[3,4-b]pyridine-5,7-dione (115062-74-3)

Guidance literature:

With triethylamine; 3-diphenyloxyphosphinyl-2-oxazolidinone; In acetonitrile; at 40 ℃; for 0.75h;

DOI:10.1016/j.ejmech.2006.12.003

upstream raw materials:

Pyridine-2,3-dicarboxylic anhydride

2,6-dimethylaniline

2,3-pyridinedicarboximide

Refernces

• 1、 Poupaert,Hamoir,Barbeaux,Lambert,Henichart. "Anticonvulsant activity of some N-phenylphthalimide derivatives in rats and mice [1]". . p. 89 - 91. Retrieved 2007/10/02.