4,5-Dimethyl-2-(2-phenylethyl)-1,3-dioxolane

Base Information

Chemical Name:4,5-Dimethyl-2-(2-phenylethyl)-1,3-dioxolane
CAS No.:6316-64-9
Molecular Formula:C13H18O2
Molecular Weight:206.2808
Hs Code.:
NSC Number:22572
DSSTox Substance ID:DTXSID30281704

Synonyms:6316-64-9;4,5-dimethyl-2-(2-phenylethyl)-1,3-dioxolane;NSC22572;DTXSID30281704;NSC-22572

Suppliers and Price of 4,5-Dimethyl-2-(2-phenylethyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4,5-Dimethyl-2-(2-phenylethyl)-1,3-dioxolane

Chemical Property:

Vapor Pressure:0.00564mmHg at 25°C
Boiling Point:282.7°Cat760mmHg
Flash Point:131.2°C
Density:0.986g/cm³
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:206.130679813
Heavy Atom Count:15
Complexity:177

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(OC(O1)CCC2=CC=CC=C2)C

Technology Process of 4,5-Dimethyl-2-(2-phenylethyl)-1,3-dioxolane

There total 1 articles about 4,5-Dimethyl-2-(2-phenylethyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 513-85-9
2.3-butanediol

: 6316-64-9
(4R,5R)-4,5-Dimethyl-2-phenethyl-[1,3]dioxolane

Guidance literature:: Al-Fe pillared montmorillonite clay; In dichloromethane; at 60 ℃; for 8h;
DOI:10.1016/S0040-4020(97)10049-7

Reference yield: 53.0%

: 6316-64-9
(4R,5R)-4,5-Dimethyl-2-phenethyl-[1,3]dioxolane

: 762-72-1
allyl-trimethyl-silane

: 3-(1-phenethyl-3-butenyloxy)-2-butanol

Guidance literature:: With boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 3h;
DOI:10.1016/j.tet.2006.11.004

Reference yield:

: 6316-64-9
(4R,5R)-4,5-Dimethyl-2-phenethyl-[1,3]dioxolane

: methyl 3-(1,2-dimethyl-2-hydroxyethoxy)-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 53 percent / BF₃*Et₂O / acetonitrile / 3 h / 0 °C

2.1: 95 percent / imidazole / CH₂Cl₂ / 0 - 20 °C

3.1: OsO₄; NaIO₄; 2,6-lutidine / dioxane; H₂O / 0 - 20 °C

4.1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 12 h / 20 °C

4.2: 501 mg / hexane; benzene; methanol / 0 - 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; boron trifluoride diethyl etherate; In 1,4-dioxane; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tet.2006.11.004