3-Hexenoic acid, 4-benzoyl-2,6-diiodophenyl ester, (3E)-

Base Information

Chemical Name:3-Hexenoic acid, 4-benzoyl-2,6-diiodophenyl ester, (3E)-
CAS No.:403615-36-1
Molecular Formula:C19H16I2O3
Molecular Weight:546.143
Hs Code.:

Synonyms:

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Chemical Property of 3-Hexenoic acid, 4-benzoyl-2,6-diiodophenyl ester, (3E)-

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Technology Process of 3-Hexenoic acid, 4-benzoyl-2,6-diiodophenyl ester, (3E)-

There total 2 articles about 3-Hexenoic acid, 4-benzoyl-2,6-diiodophenyl ester, (3E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1577-18-0
(E)-3-hexenoic acid

: 70036-74-7
3,5-diiodo-4-hydroxybenzophenone

: 403615-36-1
(E)-hex-3-enoic acid 2,6-diiodo-4-(1-phenyl-methanoyl)-phenyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 24h;
DOI:10.1021/jo0109669

Reference yield:

: 1137-42-4
4-Hydroxybenzophenone

: 403615-36-1
(E)-hex-3-enoic acid 2,6-diiodo-4-(1-phenyl-methanoyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / potassium iodide; chloramine T / H₂O; aq. NaOH / 20 °C

2: 54 percent / CH₂Cl₂ / 24 h / 20 °C

With chloroamine-T; potassium iodide; In sodium hydroxide; dichloromethane; water;
DOI:10.1021/jo0109669

Reference yield: 78.0%

: 403615-36-1
(E)-hex-3-enoic acid 2,6-diiodo-4-(1-phenyl-methanoyl)-phenyl ester

: (E)-hex-3-enoic acid 4-benzoyl-2,6-[²H]-phenyl ester

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; deuterium; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 2.83333h; under 1064.07 Torr;
DOI:10.1021/jo0109669