10,12-Octadecadienoic acid, 9-(benzoyloxy)-, methyl ester, (9R,10E,12Z)-

Base Information

Chemical Name:10,12-Octadecadienoic acid, 9-(benzoyloxy)-, methyl ester, (9R,10E,12Z)-
CAS No.:403619-52-3
Molecular Formula:C₂₆H₃₈O₄
Molecular Weight:414.585
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10,12-Octadecadienoic acid, 9-(benzoyloxy)-, methyl ester, (9R,10E,12Z)-

Chemical Property:

Purity/Quality:

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Technology Process of 10,12-Octadecadienoic acid, 9-(benzoyloxy)-, methyl ester, (9R,10E,12Z)-

There total 4 articles about 10,12-Octadecadienoic acid, 9-(benzoyloxy)-, methyl ester, (9R,10E,12Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6084-82-8,6114-34-7,6157-02-4,10075-07-7,23324-71-2,65700-62-1,69257-16-5,96393-36-1,98524-18-6,114297-06-2
9-hydroxy-(10E,12Z)-octadecadien-1-oic acid methyl ester

: 403619-52-3
Benzoic acid (2E,4Z)-(R)-1-(7-methoxycarbonyl-heptyl)-deca-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / DMAP; Et₃N / CH₂Cl₂ / 30 h / 20 °C

2: Daisel CHIRAL OD column / hexane; propan-2-ol

With dmap; Daisel CHIRAL OD column; triethylamine; In hexane; dichloromethane; isopropyl alcohol;
DOI:10.1016/S0957-4166(01)00486-4

Reference yield:

: 868364-06-1
9-10-monoepoxy-12-octadecenoic acid

: 403619-52-3
Benzoic acid (2E,4Z)-(R)-1-(7-methoxycarbonyl-heptyl)-deca-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran; hexane / 1 h / 0 °C

1.2: 140 mg / diethyl ether

2.1: 90 percent / DMAP; Et₃N / CH₂Cl₂ / 30 h / 20 °C

3.1: Daisel CHIRAL OD column / hexane; propan-2-ol

With dmap; Daisel CHIRAL OD column; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol;
DOI:10.1016/S0957-4166(01)00486-4

Reference yield:

: 186792-27-8
9,10-epoxy-(12Z)-octadecen-1-oic acid methyl ester

: 403619-52-3
Benzoic acid (2E,4Z)-(R)-1-(7-methoxycarbonyl-heptyl)-deca-2,4-dienyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 0.5 N LiOH / dioxane; H₂O / 24 h / 20 °C

2.1: LDA / tetrahydrofuran; hexane / 1 h / 0 °C

2.2: 140 mg / diethyl ether

3.1: 90 percent / DMAP; Et₃N / CH₂Cl₂ / 30 h / 20 °C

4.1: Daisel CHIRAL OD column / hexane; propan-2-ol

With dmap; lithium hydroxide; Daisel CHIRAL OD column; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; isopropyl alcohol;
DOI:10.1016/S0957-4166(01)00486-4