Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]-

Base Information

Chemical Name:Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]-
CAS No.:404010-33-9
Molecular Formula:C12H18N2O5S
Molecular Weight:302.351
Hs Code.:
DSSTox Substance ID:DTXSID80459592
Wikidata:Q82283401
Mol file:404010-33-9.mol

Synonyms:404010-33-9;Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]-;SCHEMBL6637777;DTXSID80459592;N-(5-tert-Butyl-2-methoxy-3-nitrophenyl)methanesulfonamide;MUOWODBPFRQEDV-UHFFFAOYSA-N;N-(5-(tert-butyl)-2-methoxy-3-nitrophenyl)methanesulfonamide

Suppliers and Price of Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:302.09364285
Heavy Atom Count:20
Complexity:446

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=C(C(=C1)[N+](=O)[O-])OC)NS(=O)(=O)C

Technology Process of Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]-

There total 4 articles about Methanesulfonamide, N-[5-(1,1-dimethylethyl)-2-methoxy-3-nitrophenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.4%

: 404010-31-7
5-tert-Butyl-2-methoxy-3-nitroaniline

: 404010-33-9
N-(3-nitro-5-tert-butyl-2-methoxy-phenyl)-methanesulfonamide

Guidance literature:: 5-tert-Butyl-2-methoxy-3-nitroaniline; With pyridine; methanesulfonyl chloride; In toluene; at 20 - 35 ℃;

With hydrogenchloride; In n-heptane; water; at 2 - 20 ℃; for 1.25h;

Reference yield: 87.0%

: 404010-31-7
5-tert-Butyl-2-methoxy-3-nitroaniline

: 124-63-0
methanesulfonyl chloride

: 404010-33-9
N-(3-nitro-5-tert-butyl-2-methoxy-phenyl)-methanesulfonamide

Guidance literature:: With pyridine; In toluene; at 30 - 35 ℃; Inert atmosphere;

Reference yield:

: 77055-30-2
5-tert-butyl-2-methoxy-1,3-dinitrobenzene

: 404010-33-9
N-(3-nitro-5-tert-butyl-2-methoxy-phenyl)-methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / water; methyl cyclohexane / Inert atmosphere

2: pyridine / toluene / 30 - 35 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; In water; methyl cyclohexane; toluene;