1H-Pyrrole-2-carboxylicacid,1-(cyclopropylmethyl)-4-nitro-(9CI)

Base Information

Chemical Name:1H-Pyrrole-2-carboxylicacid,1-(cyclopropylmethyl)-4-nitro-(9CI)
CAS No.:404336-13-6
Molecular Formula:C9H10N2O4
Molecular Weight:210.189
Hs Code.:
Mol file:404336-13-6.mol

Synonyms:1-cyclopropylmethyl-4-nitro-1H-pyrrole-2-carboxylic acid;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrrole-2-carboxylicacid,1-(cyclopropylmethyl)-4-nitro-(9CI)

Chemical Property:

Melting Point:215 - 217 °C
PSA：88.05000
LogP:2.02770

Purity/Quality:

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Technology Process of 1H-Pyrrole-2-carboxylicacid,1-(cyclopropylmethyl)-4-nitro-(9CI)

There total 2 articles about 1H-Pyrrole-2-carboxylicacid,1-(cyclopropylmethyl)-4-nitro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 386252-76-2
1-cyclopropylmethyl-4-nitro-1H-pyrrole-2-carboxylic acid ethyl ester

: 404336-13-6
1-(cyclopropylmethyl)-4-nitro-1H-pyrrole-2-carboxylic acid

Guidance literature:: With sodium hydroxide; In methanol; at 50 ℃; for 2h;
DOI:10.1021/jm010375a

Reference yield:

: 5930-92-7
Ethyl 4-nitropyrrole-2-carboxylate

: 404336-13-6
1-(cyclopropylmethyl)-4-nitro-1H-pyrrole-2-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: K / dimethylformamide / 1 h / 100 °C

1.2: 80 percent / KI / dimethylformamide / 5 h / 80 °C

2.1: 90 percent / aq. NaOH / ethanol / 2 h / Heating

With sodium hydroxide; potassium; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm031089x