BOMIN-1

Base Information

• Chemical Name: BOMIN-1
• CAS No.: 4081-22-5
• Molecular Formula: C9H11O4P
• Molecular Weight: 214.15500
• Mol file: 4081-22-5.mol

Synonyms:2-Ethoxy-4H-1,3,2-benzodioxaphosphorin-2-oxid;2-Ethoxy-2-oxo-3H-1,4,2-benzodioxaphosphorine;2-Ethoxy-4H-1,3,2-benzodioxaphosphoran-2-on;

Chemical Property of BOMIN-1

Chemical Property:

• Boiling Point: 269.9±33.0 °C(Predicted)
• PSA: 54.57000
• Density: 1.29±0.1 g/cm3(Predicted)
• LogP: 2.64490

Purity/Quality:

95% ^*data from raw suppliers

2-ETHOXY-2-OXO-3H-1,4,2-BENZODIOXAPHOSPHORINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BOMIN-1

There total 3 articles about BOMIN-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

salicylic alcohol (90-01-7) → 2-Ethoxy-4H-1,3,2-benzodioxaphosphoran-2-on (4081-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus oxychloride; triethylamine / CH₂Cl₂

2: triethylamine

With triethylamine; trichlorophosphate; In dichloromethane; 1: Cyclization / 2: Esterification;

DOI:10.1021/tx00050a011

Reference yield:

ethanol (64-17-5) + 2-chloro-4H-benzo[d][1,3,2]dioxaphosphinine 2-oxide (127164-51-6) → 2-Ethoxy-4H-1,3,2-benzodioxaphosphoran-2-on (4081-22-5)

Guidance literature:

With triethylamine;

DOI:10.1021/tx00050a011

Reference yield:

→ 2-Ethoxy-4H-1,3,2-benzodioxaphosphoran-2-on (4081-22-5)

Guidance literature:

2-Hydroxy-benzylalkohol, /BRN= 506857/;

upstream raw materials:

ethanol

2-chloro-4H-benzo[d][1,3,2]dioxaphosphinine 2-oxide

salicylic alcohol

Refernces