1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene]

Base Information

Chemical Name:1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene]
CAS No.:41424-40-2
Molecular Formula:C20H16S2
Molecular Weight:320.479
Hs Code.:
DSSTox Substance ID:DTXSID701191354
Nikkaji Number:J2.156.575J

Synonyms:DTXSID701191354;41424-40-2;1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene]

Suppliers and Price of 1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene]

Chemical Property:

XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:320.06934286
Heavy Atom Count:22
Complexity:332

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=CSC2=CC=CC=C2)SC3=CC=CC=C3
Isomeric SMILES:C1=CC=C(C=C1)/C(=C/SC2=CC=CC=C2)/SC3=CC=CC=C3

Technology Process of 1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene]

There total 13 articles about 1,1'-[[(1Z)-1-Phenyl-1,2-ethenediyl]bis(thio)]bis[benzene] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 35460-31-2
(2-phenylsulfanylethynyl)benzene

: 108-98-5
thiophenol

: 41424-40-2
(Z)-(1-phenylethene-1,2-diyl)bis(phenylsulfane)

Guidance literature:: With cesium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 3h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/cjoc.201190154

Reference yield: 87.0%

: 66003-76-7
Diphenyliodonium triflate

: 536-74-3
phenylacetylene

: 41424-40-2
(Z)-(1-phenylethene-1,2-diyl)bis(phenylsulfane)

Guidance literature:: With potassium sulfide; NHC-Pd(II)-Im; 3-(2-hydroxyethyl)-1-methyl-1H-imidazol-3-ium chloride; In toluene; at 80 ℃; for 12h; Reagent/catalyst; regioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/adsc.201701417