6-Methoxy-2-Methylindole-3-carboxaldehyde

Base Information

Chemical Name:6-Methoxy-2-Methylindole-3-carboxaldehyde
CAS No.:4147-43-7
Molecular Formula:C11H11NO2
Molecular Weight:189.21100
Hs Code.:2933990090
Mol file:4147-43-7.mol

Synonyms:1,2,4-Triazin-3-amine,6-methoxy-N,N-dimethyl;6-methoxy-2-methyl-indole-3-carbaldehyde;6-Methoxy-3-dimethylamino-1,2,4-triazine;6-Methoxy-2-methyl-indol-3-carboxaldehyd;formyl-3 methoxy-6 methyl-2 indole;6-Methoxy-2-methylindole-3-carboxaldehyde;6-methoxy-3-formyl-2-methylindole;

Suppliers and Price of 6-Methoxy-2-Methylindole-3-carboxaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
6-methoxy-2-methyl-1H-Indole-3-carboxaldehyde 97.00%
25G
$ 5120.00

Total 4 raw suppliers

Chemical Property of 6-Methoxy-2-Methylindole-3-carboxaldehyde

Chemical Property:

PSA：42.09000
LogP:2.29740

Purity/Quality:

98% ^*data from raw suppliers

6-methoxy-2-methyl-1H-Indole-3-carboxaldehyde 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Methoxy-2-Methylindole-3-carboxaldehyde

There total 7 articles about 6-Methoxy-2-Methylindole-3-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1968-13-4
2-methyl-6-methoxy-1H-indole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 4147-43-7
6-methoxy-2-methylindole-3-carboxaldehyde

Guidance literature:: With trichlorophosphate; at 35 ℃; for 1h;
DOI:10.1016/0223-5234(89)90108-6

Reference yield:

: 113352-66-2
1-(4-methoxy-2-nitrophenyl)propan-2-one

: 4147-43-7
6-methoxy-2-methylindole-3-carboxaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / Raney-Ni / ethyl acetate / 18 h

2: 84 percent / POCl₃ / 0.5 h / 0 °C

With hydrogen; trichlorophosphate; nickel; In ethyl acetate;
DOI:10.1021/ja00215a039

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 4147-43-7
6-methoxy-2-methylindole-3-carboxaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / cc. H₂SO₄, isoamyl nitrite / ethanol / 1 h / 0 °C

2: 55 percent / 0.5M HCl, LiCl / CuCl / H₂O; various solvent(s) / 5 deg C, 3.5 h. then 20 deg C, 4 h.

3: 95 percent / H₂ / Raney-Ni / ethyl acetate / 18 h

4: 84 percent / POCl₃ / 0.5 h / 0 °C

With hydrogenchloride; sulfuric acid; hydrogen; lithium chloride; trichlorophosphate; isopentyl nitrite; nickel; copper(l) chloride; In ethanol; water; ethyl acetate;
DOI:10.1021/ja00215a039