Technology Process of Benzenemethanol, a-[[(1,1-dimethylethyl)amino]methyl]-, hydrochloride
There total 3 articles about Benzenemethanol, a-[[(1,1-dimethylethyl)amino]methyl]-, hydrochloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C12H15Cl4NOSi;
With
ammonia borane;
In
diethyl ether;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
With
hydrogenchloride;
In
1,4-dioxane; tert-butyl methyl ether;
Inert atmosphere;
DOI:10.1002/chem.201500210
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrachlorosilane; N,N,N,N,N,N-hexamethylphosphoric triamide / ethyl acetate / 1 h / 0 - 5 °C / Inert atmosphere
2.1: ammonia borane / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
With
N,N,N,N,N,N-hexamethylphosphoric triamide; ammonia borane; tetrachlorosilane;
In
diethyl ether; ethyl acetate;
1.1: |Passerini Condensation;
DOI:10.1002/chem.201500210
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrachlorosilane; N,N,N,N,N,N-hexamethylphosphoric triamide / ethyl acetate / 1 h / 0 - 5 °C / Inert atmosphere
2.1: ammonia borane / diethyl ether / 3 h / 0 - 20 °C / Inert atmosphere
2.2: Inert atmosphere
With
N,N,N,N,N,N-hexamethylphosphoric triamide; ammonia borane; tetrachlorosilane;
In
diethyl ether; ethyl acetate;
1.1: |Passerini Condensation;
DOI:10.1002/chem.201500210
