2,3,4,5-Tetrachloro-6-methoxybenzenamine

Base Information

• Chemical Name: 2,3,4,5-Tetrachloro-6-methoxybenzenamine
• CAS No.: 42138-72-7
• Molecular Formula: C7H5Cl4NO
• Molecular Weight: 260.93300
• Mol file: 42138-72-7.mol

Synonyms:3,4,5,6-tetrachloro-2-methoxyaniline;Tetrachlor-o-anisidin;2,3,4,5-Tetrachlor-6-methoxy-anilin;2,3,4,5-tetrachloro-6-methoxy-aniline;3.4.5.6-Tetrachlor-2-amino-anisol;3.4.5.6-Tetrachlor-o-anisidin;2,3,4,5-Tetrachloro-6-methoxybenzenamine;Benzenamine,2,3,4,5-tetrachloro-6-methoxy;

Chemical Property of 2,3,4,5-Tetrachloro-6-methoxybenzenamine

Chemical Property:

• PSA: 35.25000
• LogP: 4.47220

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3,4,5-Tetrachloro-6-methoxybenzenamine

There total 11 articles about 2,3,4,5-Tetrachloro-6-methoxybenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,5-trichloro-6-methoxyaniline (66015-90-5) → Tetrachlor-o-anisidin (42138-72-7)

Guidance literature:

With chloroform; chlorine; Erwaermen des Reaktionsprodukts mit Schwefelsaeure;

DOI:10.1039/jr9430000235

Reference yield:

2-methoxyacetanilide (93-26-5) → Tetrachlor-o-anisidin (42138-72-7)

Guidance literature:

Multi-step reaction with 2 steps

1: glacial acetic acid; chlorine

2: alcoholic KOH-solution

With potassium hydroxide; chlorine; acetic acid;

Reference yield:

1,2,4,5-tetrachlorobenzene (95-94-3) → Tetrachlor-o-anisidin (42138-72-7)

Guidance literature:

Multi-step reaction with 5 steps

1: methanol. NaOH / 160 °C

2: NaOH

3: HNO₃ / 5 - 10 °C

4: acetic acid; aqueous ethanol; iron

5: chloroform; chlorine / Erwaermen des Reaktionsprodukts mit Schwefelsaeure

With sodium hydroxide; ethanol; chloroform; nitric acid; chlorine; iron; acetic acid;

DOI:10.1039/jr9430000235

upstream raw materials:

2,3,5-trichloro-6-methoxyaniline

3,4,5,6-tetrachloro-2-methoxyacetanilide

3,4,5,6-Tetrachlor-2-fluor-anilin

sodium methylate

Downstream raw materials:

2-bromo-3,4,5,6-tetrachloro-anisole

2,3,4,5-tetrachloro-6-iodo-anisole