Octanamide, N-octyl-

Base Information

• Chemical Name: Octanamide, N-octyl-
• CAS No.: 42886-89-5
• Molecular Formula: C16H33NO
• Molecular Weight: 255.444
• Mol file: 42886-89-5.mol

Synonyms:

Chemical Property of Octanamide, N-octyl-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Octanamide, N-octyl-

There total 6 articles about Octanamide, N-octyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

Octanoic acid (124-07-2) → n-Octylamine (111-86-4) + octane (111-65-9) + n-dioctylamine (1120-48-5) + Octansaeure-N-octylamid (42886-89-5) + n-octanamide (629-01-6)

Guidance literature:

Octanoic acid; With cyclopentyl methyl ether; ammonia; at 200 ℃; under 4500.45 Torr; Sealed tube; Green chemistry;

With cyclopentyl methyl ether; ammonia; hydrogen; at 200 ℃; for 6.5h; under 42004.2 Torr; Reagent/catalyst; Cooling with ice; Green chemistry;

DOI:10.1039/d0gc01441a

Reference yield: 76.0%

methyl octanate (111-11-5) → n-Octylamine (111-86-4) + octane (111-65-9) + n-dioctylamine (1120-48-5) + Octansaeure-N-octylamid (42886-89-5) + n-octanamide (629-01-6)

Guidance literature:

methyl octanate; With cyclopentyl methyl ether; ammonia; at 200 ℃; under 4500.45 Torr; Sealed tube; Green chemistry;

With cyclopentyl methyl ether; ammonia; hydrogen; at 200 ℃; for 6.5h; under 42004.2 Torr; Cooling with ice; Green chemistry;

DOI:10.1039/d0gc01441a

Reference yield: 11.0%

n-dioctylamine (1120-48-5) → Octanoic acid (124-07-2) + Octansaeure-N-octylamid (42886-89-5) + octanoyloxymethyl octanoate (76058-01-0)

Guidance literature:

With benzyl(triethyl)ammoniumpermanganate; In dichloromethane;

upstream raw materials:

chloro-dioctyl-amine

acetic anhydride

n-Octylamine

tricaprilin

Downstream raw materials:

n-Octylamine

octanol

Octanoic acid

Refernces

• 1、 Jin, Xiongjie,Kataoka, Kengo,Yatabe, Takafumi,Yamaguchi, Kazuya,Mizuno, Noritaka. "Supported Gold Nanoparticles for Efficient α-Oxygenation of Secondary and Tertiary Amines into Amides". supporting information. p. 7212 - 7217. Retrieved 2016/07/06.
• 2、 Schmidt, H.-Juergen,Schaefer, Hans J.. "Oxidation von Aminen mit Benzyl(triethyl)ammonium-permanganat". . p. 124 - 125. Retrieved 2007/10/02.