Butanal, 2-[[(4-methoxyphenyl)methoxy]methyl]-, (2S)-

Base Information

Chemical Name:Butanal, 2-[[(4-methoxyphenyl)methoxy]methyl]-, (2S)-
CAS No.:443284-63-7
Molecular Formula:C13H18O3
Molecular Weight:222.284
Hs Code.:

Synonyms:

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Chemical Property of Butanal, 2-[[(4-methoxyphenyl)methoxy]methyl]-, (2S)-

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Technology Process of Butanal, 2-[[(4-methoxyphenyl)methoxy]methyl]-, (2S)-

There total 4 articles about Butanal, 2-[[(4-methoxyphenyl)methoxy]methyl]-, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 443284-47-7
(R)-2-(4-methoxybenzyloxymethyl)butan-1-ol

: 443284-63-7
(S)-2-(4-Methoxy-benzyloxymethyl)-butyraldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1016/S0957-4166(02)00009-5

Reference yield:

: 2612-29-5
2-ethyl-1,3-propandiol

: 443284-63-7
(S)-2-(4-Methoxy-benzyloxymethyl)-butyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1 h / 0 °C

1.2: 80 percent / tetrabutylammonium iodide / tetrahydrofuran / 2 h / 20 °C

2.1: lipase from Candida rugosa / diisopropyl ether / 9 h / 20 °C

3.1: 85 percent / oxalyl chloride; DMSO / CH₂Cl₂ / 1 h / -78 °C

With oxalyl dichloride; lipase from Candida rugosa; sodium hydride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; di-isopropyl ether; 3.1: Swern oxidation;
DOI:10.1016/S0957-4166(02)00009-5

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 443284-63-7
(S)-2-(4-Methoxy-benzyloxymethyl)-butyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1 h / 0 °C

1.2: 80 percent / tetrabutylammonium iodide / tetrahydrofuran / 2 h / 20 °C

2.1: lipase from Candida rugosa / diisopropyl ether / 9 h / 20 °C

3.1: 85 percent / oxalyl chloride; DMSO / CH₂Cl₂ / 1 h / -78 °C

With oxalyl dichloride; lipase from Candida rugosa; sodium hydride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; di-isopropyl ether; 3.1: Swern oxidation;
DOI:10.1016/S0957-4166(02)00009-5