Silane, (1,1-dimethylethyl)[[(5R)-5-[(4-methoxyphenyl)methoxy]-3,6-dodecadiyn yl]oxy]diphenyl-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)[[(5R)-5-[(4-methoxyphenyl)methoxy]-3,6-dodecadiyn yl]oxy]diphenyl-
CAS No.:443285-45-8
Molecular Formula:C36H44O3Si
Molecular Weight:552.829
Hs Code.:

Synonyms:

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Chemical Property of Silane, (1,1-dimethylethyl)[[(5R)-5-[(4-methoxyphenyl)methoxy]-3,6-dodecadiyn yl]oxy]diphenyl-

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Technology Process of Silane, (1,1-dimethylethyl)[[(5R)-5-[(4-methoxyphenyl)methoxy]-3,6-dodecadiyn yl]oxy]diphenyl-

There total 2 articles about Silane, (1,1-dimethylethyl)[[(5R)-5-[(4-methoxyphenyl)methoxy]-3,6-dodecadiyn yl]oxy]diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 342902-95-8
1-(4-O-tert-butyldiphenylsilyl-1-butynyl)-(1R)-2-octynyl alcohol

: 443285-45-8
tert-butyl-[5-(4-methoxy-benzyloxy)-dodeca-3,6-diynyloxy]-diphenyl-silane

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; cyclohexane;
DOI:10.1016/S0957-4166(02)00009-5

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 443285-45-8
tert-butyl-[5-(4-methoxy-benzyloxy)-dodeca-3,6-diynyloxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / diethyl ether / 0.5 h / 20 °C

1.2: diethyl ether / 4 h / 0 - 20 °C

2.1: 86 percent / CSA / cyclohexane; CH₂Cl₂

With camphor-10-sulfonic acid; sodium hydride; In diethyl ether; dichloromethane; cyclohexane;
DOI:10.1016/S0957-4166(02)00009-5