pentan-3-yl prop-2-enoate

Base Information

Chemical Name:pentan-3-yl prop-2-enoate
CAS No.:4513-35-3
Molecular Formula:C8H14O2
Molecular Weight:142.198
Hs Code.:

Synonyms:

Suppliers and Price of pentan-3-yl prop-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of pentan-3-yl prop-2-enoate

Chemical Property:

Vapor Pressure:2.079mmHg at 25°C

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of pentan-3-yl prop-2-enoate

There total 1 articles about pentan-3-yl prop-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 584-02-1
2-pentanol

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 3852-09-3
methyl 3-methoxypropionate

: 4513-35-3
sec-Amyl acrylate

: 112032-52-7
3-Methoxy-propionic acid 1-ethyl-propyl ester

Guidance literature:: With n-butyllithium; bis(acetylacetonate)nickel(II); In benzene; at 90 ℃; for 5h; Product distribution; other temp., other time;

Reference yield:

: 4513-35-3
sec-Amyl acrylate

: 129277-94-7
2-Methyl-2E-pentanoic acid 3-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 1,4-diazabicyclo<2.2.2>octane (DABO) / 4 h / 50 °C / 3750300 Torr

2: 15 percent Chromat_. / Cp₂ZrCl₂, NaAlH₂(OCH₂CH₂OMe)2 / tetrahydrofuran; toluene / 1 h / -78 °C

With 1,4-diaza-bicyclo[2.2.2]octane; zirconocene dichloride; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; toluene;
DOI:10.1007/BF00960333

Reference yield:

: 4513-35-3
sec-Amyl acrylate

: 114607-20-4,114715-56-9,122798-52-1,122798-53-2,122798-54-3,124753-52-2,129314-00-7,129314-02-9
1-ethylpropyl (2SR,3RS)-3-hydroxy-2-methylpentanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 44 percent / DABCO / acetonitrile / 192 h / sonicated

2: 78 percent / imidazole / dimethylformamide / 16 h / 20 °C

3: H₂ / 5 percent Pd/C / ethyl acetate / 16 h / 20 °C

4: 80 percent / 48 percent HF / acetonitrile / 1 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; 1H-imidazole; hydrogen fluoride; hydrogen; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1: Baylis-Hillman reaction;
DOI:10.1016/S0040-4020(01)00647-0