1-Heptyloctylbenzene

Base Information

• Chemical Name: 1-Heptyloctylbenzene
• CAS No.: 4534-60-5
• Molecular Formula: C21H36
• Molecular Weight: 288.51100
• Mol file: 4534-60-5.mol

Synonyms:8-Phenylpentadecan;(1-Heptyl-octyl)-benzene;diheptylphenylmethane;

Chemical Property of 1-Heptyloctylbenzene

Chemical Property:

• Vapor Pressure: 2.3E-05mmHg at 25°C
• Boiling Point: 113 - 114 °C (0.04 mmHg)
• PSA: 0.00000
• LogP: 7.49120

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Heptyloctylbenzene

There total 6 articles about 1-Heptyloctylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

1-Iodoheptane (4282-40-0) + benzaldehyde (100-52-7) → 1-heptyl-1-phenyloctane (4534-60-5)

Guidance literature:

1-Iodoheptane; With chloro-trimethyl-silane; ethylene dibromide; zinc; In tetrahydrofuran; at 35 - 40 ℃; for 12h;

benzaldehyde; With bis(acetylacetonate)nickel(II); chloro-trimethyl-silane; triethylamine; In tetrahydrofuran; at -18 - 20 ℃;

DOI:10.1016/j.tet.2008.09.066

Reference yield:

diheptylphenyl carbinol (67267-89-4) → 1-heptyl-1-phenyloctane (4534-60-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In perchloric acid; acetic acid; under 2942.03 Torr;

Reference yield:

n-octanophenone (1674-37-9) → 1-heptyl-1-phenyloctane (4534-60-5)

Guidance literature:

Multi-step reaction with 2 steps

2: H₂ / 5percent Pd/C / acetic acid; HClO₄ / 2942.03 Torr

With hydrogen; palladium on activated charcoal; In perchloric acid; acetic acid;

upstream raw materials:

diheptylphenyl carbinol

n-octanophenone

n-octanoic acid chloride

benzene

Refernces

• 1、 Mikulski, R.,Czerniawski, M.,Kampert, M.,Zielinska, J.. "COLLOIDAL PROPERTIES OF SODIUM 4-BENZENESULFONATE WITH REFERENCE TO PETROLEUM RECOVERY". . p. 165 - 173. Retrieved 2007/10/02.