Ccris 3572

Base Information

Chemical Name:Ccris 3572
CAS No.:97135-11-0
Molecular Formula:C₂₁H₁₅NO₃
Molecular Weight:329.355
Hs Code.:
DSSTox Substance ID:DTXSID10914164
Wikidata:Q82884918

Synonyms:97135-11-0;CCRIS 3572;anti-(+-)-Dibenz(a,h)acridine-10,11-diol-8,9-epoxide;DTXSID10914164;3-Hydroxybenzo[a][1]benzoxireno[2,3-h]acridin-2(13H)-one;ANTI-(+/-)-DIBENZ[A,H]ACRIDINE-10,11-DIOL-8,9-EPOXIDE

Suppliers and Price of Ccris 3572

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of Ccris 3572

Chemical Property:

Vapor Pressure:1.33E-22mmHg at 25°C
Boiling Point:733.7°Cat760mmHg
Flash Point:397.6°C
Density:1.61g/cm³
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:325.07389321
Heavy Atom Count:25
Complexity:870

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C=C4C=CC5=C(C(=O)C6=C(C5=C4N3)O6)O

Technology Process of Ccris 3572

There total 9 articles about Ccris 3572 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 97135-18-7,110927-22-5
(+/-)-trans-10,11-dihydroxy-10,11-dihydrodibenzyacridine

: 97135-11-0
(+/-)-10α,11β-dihydroxy-8α,9α-epoxy-8,9,10,11-tetrahydrodibenz(a,h)acridine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1021/jo00217a011

Reference yield:

: 97135-12-1
8,9,10,11-tetrahydrodibenzacridine

: 97135-11-0
(+/-)-10α,11β-dihydroxy-8α,9α-epoxy-8,9,10,11-tetrahydrodibenz(a,h)acridine

Guidance literature:: Multi-step reaction with 8 steps

1: acetic acid / 28 h / Heating

2: 65 percent / I₂ / benzene / 15 h / Heating

3: 90 percent / 30percent aq. NaOH / tetrahydrofuran; methanol / 2.5 h / Ambient temperature

4: 90 percent / pyridine / 18 h / Ambient temperature

5: 97 percent / N-bromosuccinimide, α,α'-azobis(isobutyrodinitrile) / CCl4 / 0.25 h / 63 - 65 °C

6: 71 percent / Li₂CO₃, LIF, HMPA / 3 h / 85 - 90 °C

7: 70 percent / NH₃ gas, / tetrahydrofuran; methanol / 2.5 h / Ambient temperature

8: 48 percent / m-chloroperoxybenzoic acid / tetrahydrofuran / 1 h / Ambient temperature

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonia; iodine; lithium carbonate; lithium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; tetrachloromethane; acetic acid; benzene;
DOI:10.1021/jo00217a011

Reference yield:

: 97135-19-8,102421-97-6,140460-94-2,140460-95-3
(+/-)-trans-(10,11)-dihydroxy-8,9,10,11-tetrahydrodibenzacridine

: 97135-11-0
(+/-)-10α,11β-dihydroxy-8α,9α-epoxy-8,9,10,11-tetrahydrodibenz(a,h)acridine

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / pyridine / 18 h / Ambient temperature

2: 97 percent / N-bromosuccinimide, α,α'-azobis(isobutyrodinitrile) / CCl4 / 0.25 h / 63 - 65 °C

3: 71 percent / Li₂CO₃, LIF, HMPA / 3 h / 85 - 90 °C

4: 70 percent / NH₃ gas, / tetrahydrofuran; methanol / 2.5 h / Ambient temperature

5: 48 percent / m-chloroperoxybenzoic acid / tetrahydrofuran / 1 h / Ambient temperature

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); ammonia; lithium carbonate; lithium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; tetrachloromethane;
DOI:10.1021/jo00217a011