1-METHYL-2-(PHENYLSULFANYL)-1H-IMIDAZOLE-5-CARBALDEHYDE

Base Information

Chemical Name:1-METHYL-2-(PHENYLSULFANYL)-1H-IMIDAZOLE-5-CARBALDEHYDE
CAS No.:460990-29-8
Molecular Formula:C11H10N2OS
Molecular Weight:218.279
Hs Code.:
Mol file:460990-29-8.mol

Synonyms:5-formyl-1-methyl-2-phenylsulfanyl-1H-imidazole;3-Methyl-2-phenylsulfanyl-3H-imidazole-4-carbaldehyde;1-methyl-2-phenylsulfanyl-1H-imidazole-4-carboxaldehyde;

Suppliers and Price of 1-METHYL-2-(PHENYLSULFANYL)-1H-IMIDAZOLE-5-CARBALDEHYDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-METHYL-2-(PHENYLSULFANYL)-1H-IMIDAZOLE-5-CARBALDEHYDE

Chemical Property:

Melting Point:57 - 58 °C (hexane)
PSA：60.19000
LogP:2.38380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 1-METHYL-2-(PHENYLSULFANYL)-1H-IMIDAZOLE-5-CARBALDEHYDE

There total 2 articles about 1-METHYL-2-(PHENYLSULFANYL)-1H-IMIDAZOLE-5-CARBALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 79487-95-9
1-methyl-2-phenylsulfanyl-1H-imidazole

: 460990-29-8
3-methyl-2-phenylsulfanylimidazole-4-carbaldehyde

Guidance literature:: With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; 1,2-dimethoxyethane; at -78 ℃;
DOI:10.1016/S0040-4039(02)00782-7

Reference yield: 80.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 460990-29-8
3-methyl-2-phenylsulfanylimidazole-4-carbaldehyde

Guidance literature:: 1-methyl-2-phenylsulfanyl-1H-imidazole; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; for 0.25h;

N,N-dimethyl-formamide; In tetrahydrofuran; hexanes; at -78 - 20 ℃; for 1.16667h;

With water; ammonium chloride; In tetrahydrofuran; hexanes; ethyl acetate;

Reference yield: 97.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 460990-29-8
3-methyl-2-phenylsulfanylimidazole-4-carbaldehyde

: 940962-59-4
5-[2-(ethoxycarbonyl)ethenyl]-1-methyl-2-phenylsulfanyl-1H-imidazole

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 0 - 20 ℃; for 5h;
DOI:10.1016/j.tet.2006.08.027