10-Oxa-2,5,8-triazadodecanoic acid, 5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl] amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl- 9-oxo-, 1,1-dimethylethyl ester

Base Information

Chemical Name:10-Oxa-2,5,8-triazadodecanoic acid, 5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl] amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl- 9-oxo-, 1,1-dimethylethyl ester
CAS No.:465512-97-4
Molecular Formula:C48H66N4O12
Molecular Weight:891.072
Hs Code.:

10-Oxa-2,5,8-triazadodecanoic acid,
5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl]
amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl-
9-oxo-, 1,1-dimethylethyl ester

Synonyms:

Suppliers and Price of 10-Oxa-2,5,8-triazadodecanoic acid, 5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl] amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl- 9-oxo-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-Oxa-2,5,8-triazadodecanoic acid, 5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl] amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl- 9-oxo-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-Oxa-2,5,8-triazadodecanoic acid, 5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl] amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl- 9-oxo-, 1,1-dimethylethyl ester

There total 4 articles about 10-Oxa-2,5,8-triazadodecanoic acid, 5-[2-[[(1,1-dimethylethoxy)carbonyl][[4-(methoxycarbonyl)phenyl]methyl] amino]ethyl]-2,8-bis[[4-(methoxycarbonyl)phenyl]methyl]-11,11-dimethyl- 9-oxo-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 465512-96-3
N,N,N-tris{2-[(4-metoxycarbonylphenyl)methylamino]ethyl}amine

: 465512-97-4
N,N,N-tris{2-[(4-metoxycarbonylphenyl)methyl(tert-butoxycarbonyl)amino]ethyl}amine

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1002/1521-3765(20020617)8:12<2753::AID-CHEM2753>3.0.CO;2-4

Reference yield:

: 1129-35-7
4-cyanobenzoic acid methyl ester

: 465512-97-4
N,N,N-tris{2-[(4-metoxycarbonylphenyl)methyl(tert-butoxycarbonyl)amino]ethyl}amine

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / SnCl₂; HCl / diethyl ether / 48 h

2: 85 percent / acetonitrile / 4 h

3: 99 percent / NaBH₄ / methanol / 0 - 20 °C

4: 69 percent / CH₂Cl₂ / 20 °C

With hydrogenchloride; sodium tetrahydroborate; tin(ll) chloride; In methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1002/1521-3765(20020617)8:12<2753::AID-CHEM2753>3.0.CO;2-4

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 465512-97-4
N,N,N-tris{2-[(4-metoxycarbonylphenyl)methyl(tert-butoxycarbonyl)amino]ethyl}amine

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / acetonitrile / 4 h

2: 99 percent / NaBH₄ / methanol / 0 - 20 °C

3: 69 percent / CH₂Cl₂ / 20 °C

With sodium tetrahydroborate; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/1521-3765(20020617)8:12<2753::AID-CHEM2753>3.0.CO;2-4