Phosphonic dichloride, (1-methylpropyl)-

Base Information

• Chemical Name: Phosphonic dichloride, (1-methylpropyl)-
• CAS No.: 4707-94-2
• Molecular Formula: C4H9Cl2OP
• Molecular Weight: 174.995
• Mol file: 4707-94-2.mol

Synonyms:

Chemical Property of Phosphonic dichloride, (1-methylpropyl)-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphonic dichloride, (1-methylpropyl)-

There total 2 articles about Phosphonic dichloride, (1-methylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

n-butane (106-97-8,9003-29-6,9021-92-5) → butylphosphonic dichloride (2302-80-9) + sec-Butylphosphonic dichloride (4707-94-2)

Guidance literature:

With oxygen; phosphorus trichloride; at -20 - -15 ℃;

Reference yield:

n-butane (106-97-8,9003-29-6,9021-92-5) + phosphorus trichloride (7719-12-2,52843-90-0) → butylphosphonic dichloride (2302-80-9) + sec-Butylphosphonic dichloride (4707-94-2)

Guidance literature:

at -15 ℃;

DOI:10.1592/phco.21.7.767.34577

Reference yield: 87.5%

sec-Butylphosphonic dichloride (4707-94-2) + para-tert-butylphenol (98-54-4) → sec-butyl-phosphonic acid bis-(4-tert-butyl-phenyl) ester

Guidance literature:

With triethylamine; In benzene; at 65 - 70 ℃; for 10h;

DOI:10.1002/(SICI)1096-9063(199706)50:2<85::AID-PS576>3.0.CO;2-E

upstream raw materials:

n-butane

phosphorus trichloride