4-N-OCTANOYLBIPHENYL

Base Information

• Chemical Name: 4-N-OCTANOYLBIPHENYL
• CAS No.: 47162-00-5
• Molecular Formula: C20H24O
• Molecular Weight: 280.41
• Hs Code.: 2914399090
• Mol file: 47162-00-5.mol

Synonyms:1-biphenyl-4-yl-octan-1-one;4-n-Octanoylbiphenyl;4-Heptyl-biphenyl-keton;4-Octanoyl-biphenyl;

Chemical Property of 4-N-OCTANOYLBIPHENYL

Chemical Property:

• Vapor Pressure: 6.12E-07mmHg at 25°C
• Melting Point: 100oC
• Boiling Point: 200oC / 3mmHg
• Flash Point: 176.3oC
• PSA: 17.07000
• Density: 0.982g/cm3
• LogP: 5.89680
• Solubility.: almost transparency in Toluene

Purity/Quality:

98%,99%, ^*data from raw suppliers

4-n-Octanoylbiphenyl ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-N-OCTANOYLBIPHENYL

There total 2 articles about 4-N-OCTANOYLBIPHENYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

biphenyl (92-52-4,1594-86-1) + n-octanoic acid chloride (111-64-8) → 1-biphenyl-4-yl-octan-1-one (47162-00-5)

Guidance literature:

With aluminium trichloride;

Reference yield:

→ 1-biphenyl-4-yl-octan-1-one (47162-00-5)

Guidance literature:

Biphenyl, Octanoylchlorid, Nitrobenzol, AlCl3 (50grad);

Reference yield:

1-biphenyl-4-yl-octan-1-one (47162-00-5) → 4-octyl-4'-cyanobiphenyl (52709-84-9,121479-48-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h

2: 1) TiCl₄, 2) hydroxylamine hydrochloride, pyridine / 1) CH₂Cl₂, 0 deg C, 30 min, 2) ethanol, reflux, 2 h

3: 83 percent / acetic anhydride / 2 h / Heating

With pyridine; potassium hydroxide; hydroxylamine hydrochloride; acetic anhydride; titanium tetrachloride; hydrazine hydrate;

upstream raw materials:

biphenyl

n-octanoic acid chloride

Downstream raw materials:

4-octyl-1,1′-biphenyl

4-octyl-4'-cyanobiphenyl

Refernces