1H-1,4-Benzodiazepinium, 7-chloro-2,3-dihydro-4-(2-hydroxypropyl)-2-oxo-5-phenyl-

Base Information

• Chemical Name: 1H-1,4-Benzodiazepinium, 7-chloro-2,3-dihydro-4-(2-hydroxypropyl)-2-oxo-5-phenyl-
• CAS No.: 47267-80-1
• Molecular Formula: C18H18ClN2O2
• Molecular Weight: 329.806

Synonyms:

Chemical Property of 1H-1,4-Benzodiazepinium, 7-chloro-2,3-dihydro-4-(2-hydroxypropyl)-2-oxo-5-phenyl-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-1,4-Benzodiazepinium, 7-chloro-2,3-dihydro-4-(2-hydroxypropyl)-2-oxo-5-phenyl-

There total 2 articles about 1H-1,4-Benzodiazepinium, 7-chloro-2,3-dihydro-4-(2-hydroxypropyl)-2-oxo-5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxazolam (24143-17-7) → 2-(4b-hydroxyisopropylamino)acetanilide-5-chlorobenzophenone (24111-57-7) + 7-Chloro-4-(2-hydroxy-propyl)-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-4-ium (47267-80-1) + 5-chloro-2-aminobenzophenone (719-59-5)

Guidance literature:

With hydrogen; In dimethylsulfoxide-d6; for 96h; Mechanism; Thermodynamic data; variation of pH, ionic strength, temperatute; δH excit, ΔE excit, ΔS excit, ΔG excit;

DOI:10.1248/cpb.32.1080

Reference yield:

oxazolam (24143-17-7) → 7-Chloro-4-(2-hydroxy-propyl)-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-4-ium (47267-80-1)

Guidance literature:

With hydrogenchloride; In ethanol; water; Equilibrium constant; Mechanism; variation of pH and buffers.;

DOI:10.1248/cpb.30.3810

Reference yield:

7-Chloro-4-(2-hydroxy-propyl)-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-4-ium (47267-80-1) → oxazolam (24143-17-7)

Guidance literature:

With borate buffer (pH=8-10.5); In ethanol; water; Equilibrium constant; Mechanism; variation of pH and buffers.;

DOI:10.1248/cpb.30.3810

upstream raw materials:

oxazolam

Downstream raw materials:

oxazolam

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