Phosphinic acid, (4-ethoxyphenyl)-4-pentenyl-, 4-pentenyl ester

Base Information

Chemical Name:Phosphinic acid, (4-ethoxyphenyl)-4-pentenyl-, 4-pentenyl ester
CAS No.:473000-56-5
Molecular Formula:C₁₈H₂₇O₃P
Molecular Weight:322.384
Hs Code.:

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Chemical Property of Phosphinic acid, (4-ethoxyphenyl)-4-pentenyl-, 4-pentenyl ester

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Technology Process of Phosphinic acid, (4-ethoxyphenyl)-4-pentenyl-, 4-pentenyl ester

There total 1 articles about Phosphinic acid, (4-ethoxyphenyl)-4-pentenyl-, 4-pentenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-73-1
Phenetole

: 473000-56-5
pent-4-enyl (+/-)-(4-ethoxyphenyl)(pent-4-enyl)phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 40 percent / trichlorophosphine; SnCl₄ / 72 h / Heating

2: pyridine / diethyl ether / 2 h / 20 °C

3: 120 °C

With pyridine; tin(IV) chloride; phosphorus trichloride; In diethyl ether; 3: Arbuzov reaction;
DOI:10.1016/j.bmc.2003.09.015

Reference yield:

: 473000-56-5
pent-4-enyl (+/-)-(4-ethoxyphenyl)(pent-4-enyl)phosphinate

: C₁₃H₁₈ClO₂P

Guidance literature:: With phosphorus pentachloride; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2003.09.015

Reference yield:

: 473000-56-5
pent-4-enyl (+/-)-(4-ethoxyphenyl)(pent-4-enyl)phosphinate

: ethyl (+/-)-2-(4-ethoxyphenyl)-2-oxoazaphosphoroc-6-ene-1-acetate

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅ / CH₂Cl₂ / 3 h / 20 °C

2: triethylamine / CH₂Cl₂ / 3 h

3: 35 percent / benzylidene-bis-(tricyclohexylphosphine)dichlororuthenium / CH₂Cl₂ / 2 h / Heating

With phosphorus pentachloride; triethylamine; Grubbs catalyst first generation; In dichloromethane;
DOI:10.1016/j.bmc.2003.09.015