BENZYL TRI-BENZYLGALLOATE

Base Information

• Chemical Name: BENZYL TRI-BENZYLGALLOATE
• CAS No.: 475161-97-8
• Molecular Formula: C35H30O5
• Molecular Weight: 530.62
• Mol file: 475161-97-8.mol

Synonyms:3,4,5-Tribenzyl-thiopyridazin;Benzenemethanol,3,4,5-tris[[4-(dodecyloxy)phenyl]methoxy];3,4,5-tris-benzyloxy-benzoic acid benzyl ester;Benzyl Tri-benzylgalloate;3,4,5-tris-benzylsulfanyl-pyridazine;3,4,5-Tris-benzyloxy-benzoesaeure-benzylester;3,4,5-tris[p-(dodecan-1-yloxy)benzyloxy]benzyl alcohol;3,4,5-tris[p-(n-dodecan-1-yloxy)benzyloxy]benzyl alcohol;3,4,5-Tris-benzylmercapto-pyridazin;

Chemical Property of BENZYL TRI-BENZYLGALLOATE

Chemical Property:

• Vapor Pressure: 1.5E-17mmHg at 25°C
• Melting Point: 88-90°C
• PSA: 53.99000
• LogP: 7.78060
• Solubility.: Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

97% ^*data from raw suppliers

BenzylTri-benzylgalloate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL TRI-BENZYLGALLOATE

There total 2 articles about BENZYL TRI-BENZYLGALLOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3,4,5-trihydroxybenzoic acid (149-91-7) + benzyl chloride (100-44-7) → benzyl 3,4,5-tris(benzyloxy)benzoate (475161-97-8)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 4.5h;

DOI:10.1248/cpb.c13-00458

Reference yield: 80.0%

3,4,5-trihydroxybenzoic acid (149-91-7) + benzyl bromide (100-39-0) → benzyl 3,4,5-tris(benzyloxy)benzoate (475161-97-8)

Guidance literature:

With potassium carbonate; In acetone; for 12h; Heating;

DOI:10.1002/hlca.200390053

Reference yield: 96.0%

benzyl 3,4,5-tris(benzyloxy)benzoate (475161-97-8) → 3,4,5-tribenzyloxybenzoic acid (1486-48-2)

Guidance literature:

With sodium hydroxide; In ethanol; at 80 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c6ra13075e

upstream raw materials:

3,4,5-trihydroxybenzoic acid

benzyl chloride

benzyl bromide

Downstream raw materials:

3,4,5-tribenzyloxybenzoic acid

3,4,5-tris-benzyloxy-N-(2-hydroxy-1,1-bis-hydroxymethyl-ethyl)-benzamide

pentafluorophenyl 3,4,5-tribenzyloxybenzoate

C₅₉H₅₄N₂O₉

Refernces

• 1、 Baumgarten, Kai D.,Czekelius, Constantin,Michaelis, Carina S.,Thieltges, David D. S.. "Synthesis of B-ring-fluorinated (?)-epicatechin gallate derivatives". supporting information. p. 4024 - 4028. Retrieved 2020/06/09.
• 2、 -. "1,3-benzodioxole natural salvianolic acid ester compound and blood fat reduction application thereof". Paragraph 0032; 0036-0037. . Retrieved 2019/10/17.