Benzene, 1-bromo-3-fluoro-5-(2-propenyloxy)-

Base Information

Chemical Name:Benzene, 1-bromo-3-fluoro-5-(2-propenyloxy)-
CAS No.:477956-04-0
Molecular Formula:C9H8BrFO
Molecular Weight:231.064
Hs Code.:
Mol file:477956-04-0.mol

Synonyms:

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Chemical Property of Benzene, 1-bromo-3-fluoro-5-(2-propenyloxy)-

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Technology Process of Benzene, 1-bromo-3-fluoro-5-(2-propenyloxy)-

There total 1 articles about Benzene, 1-bromo-3-fluoro-5-(2-propenyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 461-96-1
3,5-difluorobromobenzene

: 107-18-6
allyl alcohol

: 477956-04-0
1-allyloxy-3-bromo-5-fluoro-benzene

Guidance literature:: allyl alcohol; With sodium hydride; In dimethyl amine; at 20 ℃; for 1.5h;

3,5-difluorobromobenzene; In dimethyl amine; at 20 ℃;

Reference yield: 55.0%

: 875762-89-3
tert-butyl (S)-2-((tert-butyldimethylsilyloxy)methyl)aziridine-1-carboxylate

: 477956-04-0
1-allyloxy-3-bromo-5-fluoro-benzene

: 875762-90-6
C₂₃H₃₈FNO₄Si

Guidance literature:: 1-allyloxy-3-bromo-5-fluoro-benzene; With magnesium; ethylene dibromide; In tetrahydrofuran; at 20 ℃; for 0.5h;

tert-butyl (S)-2-((tert-butyldimethylsilyloxy)methyl)aziridine-1-carboxylate; copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; diethyl ether; at -40 - 20 ℃; for 72h;

With ammonium chloride; In tetrahydrofuran; diethyl ether; water;

Reference yield:

: 477956-04-0
1-allyloxy-3-bromo-5-fluoro-benzene

: 477956-22-2
2-(2,2-dimethyl-[1,3]dioxolan-4-yl)-aziridine-1-carboxylic acid tert-butyl ester

: 4-(3-alloxy-5-fluoro-phenyl)-3-amino-butane-1,2-diol

Guidance literature:: 1-allyloxy-3-bromo-5-fluoro-benzene; With copper(I) bromide dimethylsulfide complex; magnesium; In tetrahydrofuran; at -30 ℃; for 0.5h;

2-(2,2-dimethyl-[1,3]dioxolan-4-yl)-aziridine-1-carboxylic acid tert-butyl ester; In tetrahydrofuran; at -30 ℃; for 2.5h;

In methanol; at 50 ℃; for 3.5h;