5-Vanillylidene barbituric acid

Base Information

• Chemical Name: 5-Vanillylidene barbituric acid
• CAS No.: 40367-32-6
• Molecular Formula: C12H10N2O5
• Molecular Weight: 262.222
• European Community (EC) Number: 637-032-5
• NSC Number: 93945
• DSSTox Substance ID: DTXSID50415302
• Nikkaji Number: J2.216.102D
• ChEMBL ID: CHEMBL565660
• Mol file: 40367-32-6.mol

Synonyms:40367-32-6;5-Vanillylidene barbituric acid;MLS000736959;CHEMBL565660;5-[(4-hydroxy-3-methoxy-phenyl)methylidene]-1,3-diazinane-2,4,6-trione;NSC93945;5-[(4-hydroxy-3-methoxyphenyl)methylidene]-1,3-diazinane-2,4,6-trione;SCHEMBL13848480;DTXSID50415302;BDBM50497174;NSC-93945;STK325981;STL149902;AKOS000746578;AKOS005749695;SMR000528443;4-hydroxy-3-methoxybenzylidenebarbituric acid;5-(3-Methoxy-4-hydroxybenzylidene)barbituric acid;5-(4-HYDROXY-3-METHOXYBENZYLIDENE)BARBITURIC ACID;(5Z)-2,6-dihydroxy-5-(4-hydroxy-3-methoxybenzylidene)pyrimidin-4(5H)-one;5-(4-hydroxy-3-methoxybenzylidene)pyrimidine-2,4,6(1H,3H,5H)-trione;5-[(4-hydroxy-3-methoxyphenyl)methylene]-2,4,6(1H,3H,5H)-pyrimidinetrione

Chemical Property of 5-Vanillylidene barbituric acid

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.471g/cm³
• XLogP3: 0.7
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 262.05897142
• Heavy Atom Count: 19
• Complexity: 423

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: COC1=C(C=CC(=C1)C=C2C(=O)NC(=O)NC2=O)O

Technology Process of 5-Vanillylidene barbituric acid

There total 4 articles about 5-Vanillylidene barbituric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

BARBITURIC ACID (67-52-7,944357-77-1) + vanillin (121-33-5,8014-42-4) → 5-(3-methoxyl-4-hydroxybenzylidene)pyrimidine-2,4,6(1H,3H,5H)-trione (40367-32-6)

Guidance literature:

at 50 ℃; for 1h;

DOI:10.1016/S0040-4020(03)00554-4

Reference yield: 50.0%

BARBITURIC ACID (67-52-7,944357-77-1) + vanillin (121-33-5,8014-42-4) → 5-(4-hydroxy-3-methoxyphenyl)-1H,1'H-spiro[furo[2,3-d]pyrimidine-6,5'-pyrimidine]-2,2',4,4',6'(3H,3'H,5H)-pentaone (1333530-02-1) + 5-(3-methoxyl-4-hydroxybenzylidene)pyrimidine-2,4,6(1H,3H,5H)-trione (40367-32-6)

Guidance literature:

With bromocyane; L-Tartaric acid; In methanol; at 0 - 20 ℃; screw cap tube;

DOI:10.5012/bkcs.2011.32.9.3382

Reference yield:

urea- barbituric acid + vanillin (121-33-5,8014-42-4) → 5-(3-methoxyl-4-hydroxybenzylidene)pyrimidine-2,4,6(1H,3H,5H)-trione (40367-32-6)

Guidance literature:

Milling;

DOI:10.1021/acs.joc.1c01817

upstream raw materials:

BARBITURIC ACID

vanillin

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 40367-32-6 5-[(4-hydroxy-3-methoxyphenyl)methylidene]pyrimidine-2,4,6(1H,3H,5H)-trione

Send

Send

Metric Ton KG G Pound L ML

Send

Send