3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(methylthio)-1-(phenylmethyl)-1H-imidazol -5-yl]-, dimethyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(methylthio)-1-(phenylmethyl)-1H-imidazol -5-yl]-, dimethyl ester
CAS No.:479400-33-4
Molecular Formula:C₂₂H₂₅N₃O₄S
Molecular Weight:427.524
Hs Code.:
Mol file:479400-33-4.mol

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(methylthio)-1-(phenylmethyl)-1H-imidazol -5-yl]-, dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(methylthio)-1-(phenylmethyl)-1H-imidazol -5-yl]-, dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(methylthio)-1-(phenylmethyl)-1H-imidazol -5-yl]-, dimethyl ester

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-[2-(methylthio)-1-(phenylmethyl)-1H-imidazol -5-yl]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 105-45-3
acetoacetic acid methyl ester

: 479400-30-1
1-benzyl-2-(methylsulfanyl)imidazole-5-carbaldehyde

: 479400-33-4
dimethyl 1,4-dihydro-2,6,-dimethyl-4-(1-phenylmethyl-2-methylthio-5-imidazolyl)pyridine-3,5-dicarboxylate

Guidance literature:: With ammonium hydroxide; In methanol; Heating;

Reference yield:

: 3287-99-8,39110-74-2,108321-65-9
benzylamine hydrochloride

: 479400-33-4
dimethyl 1,4-dihydro-2,6,-dimethyl-4-(1-phenylmethyl-2-methylthio-5-imidazolyl)pyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 89 percent / acetic acid; butan-1-ol / 70 h

2.1: aq. NaOH / methanol / 0.17 h / 20 °C

2.2: 75 percent / methanol / 20 °C

3.1: 80 percent / MnO₂ / CHCl₃ / Heating

4.1: 30 percent / NH₄OH / methanol / Heating

With manganese(IV) oxide; ammonium hydroxide; sodium hydroxide; In methanol; chloroform; acetic acid; butan-1-ol; 4.1: Hantzch condensation;

Reference yield:

: 338414-90-7
5-hydroxymethyl-2-methylthio-1-phenylmethylimidazole

: 479400-33-4
dimethyl 1,4-dihydro-2,6,-dimethyl-4-(1-phenylmethyl-2-methylthio-5-imidazolyl)pyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / MnO₂ / CHCl₃ / Heating

2: 30 percent / NH₄OH / methanol / Heating

With manganese(IV) oxide; ammonium hydroxide; In methanol; chloroform; 2: Hantzch condensation;