2(3H)-Benzofuranone, 3-(4-methylphenyl)-

Base Information

Chemical Name:2(3H)-Benzofuranone, 3-(4-methylphenyl)-
CAS No.:4815-06-9
Molecular Formula:C15H12O2
Molecular Weight:224.259
Hs Code.:
Mol file:4815-06-9.mol

Synonyms:

Suppliers and Price of 2(3H)-Benzofuranone, 3-(4-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2(3H)-Benzofuranone, 3-(4-methylphenyl)-

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2(3H)-Benzofuranone, 3-(4-methylphenyl)-

There total 6 articles about 2(3H)-Benzofuranone, 3-(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2-(2-hydroxyphenyl)-2-p-tolylacetonitrile

: 4815-06-9
3-p-tolylbenzofuran-2(3H)-one

Guidance literature:: With hydrogenchloride; In water; acetonitrile; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1002/cjoc.201400463

Reference yield:

: 90-02-8
salicylaldehyde

: 4815-06-9
3-p-tolylbenzofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: potassium carbonate; tetrabutyl ammonium fluoride / tetrahydrofuran; acetonitrile / 12 h / 80 °C / Inert atmosphere; Schlenk technique

4: hydrogenchloride / acetonitrile; water / 12 h / 80 °C / Inert atmosphere

With hydrogenchloride; tetrabutyl ammonium fluoride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/cjoc.201400463

Reference yield:

: 2-[hydroxy(4-methylphenyl)methyl]phenol

: 4815-06-9
3-p-tolylbenzofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2: potassium carbonate; tetrabutyl ammonium fluoride / tetrahydrofuran; acetonitrile / 12 h / 80 °C / Inert atmosphere; Schlenk technique

3: hydrogenchloride / acetonitrile; water / 12 h / 80 °C / Inert atmosphere

With hydrogenchloride; tetrabutyl ammonium fluoride; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1002/cjoc.201400463